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dx.doi.org/ 10.18577/2307-6046-2015-0-11-1-1

УДК 669.017.165

Vakhromov R.O., Tkachenko E.A., Lukinа E.A., Selivanov A.A.

Influence of homogenization annealing on structure and properties of ingots from 1933 alloy of Al–Zn–Mg–Cu system

Homogenizing annealing of ingots is held to dissolve the nonequilibrium excess phases, eliminating intergranular segregation and reduce internal stresses in the ingots of aluminum alloys. Simultaneously, there is a process of disintegration of solid solution of aluminum small additions of transition metals( manganese, chromium, zirconium) to form dispersoids. The influence of different modes of homogenization on the volume fraction of nonequilibrium structural components, the properties of the 1933 alloy ingot at elevated temperatures, density of distribution and size of Al3Zr dispersoid are represented.

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Reference list

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dx.doi.org/ 10.18577/2307-6046-2015-0-11-2-2

УДК 621.791.3

Ogorodov D.V., Popov D.A., Trapeznikov A.V.

Methods of preparing аluminum-zirconium master alloy (review)

The article provides an overview of the main methods of obtaining aluminum-zirconium alloys are marked with their advantages and disadvantages. The equipment and brand materials, which are used in the manufacture of zirconium master alloys, shows the influence of the characteristics of the equipment and the selection of raw materials to the process of obtaining ligatures. The conclusions of the most promising methods of obtaining Al–Zr master alloys.

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Reference list

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dx.doi.org/ 10.18577/2307-6046-2015-0-11-3-3

УДК 669.018.95:620.178.6

Karmyshev I.E., Krasnov E.I.

The study of the technological characteristics of the formation of a composite ma-terial based on aluminum alloy using microplastic deformation

The paper presents the results of a study of the technological characteristics of the formation of a composite material based on aluminum, reinforced with discrete boron fibers. Since boron has anomalously large neutron- absorption cross- section, the coating of a composite material with the addition of boron can be used as protection against thermal neutrons of gamma detectors of the outer surface of downhole geophysical devices. With the development of new technologies equipment decreases in size, the number of devices increases and free space in which protection system is placed becomes less. The use of this material allows manufacturing protective coating with a thickness of 1,5 mm and it provides much higher attenuation of the thermal neutron flux than currently used materials with a layer thickness of 5 mm. The results of test for thermocycling of composite material samples with different volume fraction of reinforcing agent (from 30 to 50 vol. %) are shown.

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Reference list

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dx.doi.org/ 10.18577/2307-6046-2015-0-11-4-4

УДК 666.266.6

Chaynikova A.S., Vaganova M.L., Shchegoleva N.E., Lebedeva Yu.E.

Technological aspects of fabrication of radiotransparent glass-ceramic materials based on high-temperature aluminosilicate systems (review)

An analysis of state-of-art technology solutions in the area of radiotransparent glass-ceramic materials based on aluminosilicate systems was made. The development of glass-ceramic materials fabrication methods was overviewed from glass to ceramic technology. It was shown that direct controlled crystallisation performance provides fabrication of materials with unique combination of physical-mechanical, thermophysical and functional properties. The examples of sol-gel fabrication of aluminosilicate ceramics were given. Advantages and disadvantages of different technological methods used for radiotransparent pyrocerams fabrication were discussed. Technological problems of creating complex constructions made of radiotransparent pyrocerams were overviewed.

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Reference list

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dx.doi.org/ 10.18577/2307-6046-2015-0-11-5-5

УДК 667.621:678.8

Beider E.Ya., Petrova G.N.

The thermoplastic binder for polymeric composite materials

Properties of thermoplastic binder on the basis of superstructural thermoplastics are given in the article. The algorithm of actions is described at selection of binder on the basis of thermoplastics for manufacture of PCM. On example of polysulphone the influence of molecular weight on thermal-physical, mechanical and rheological properties of the thermoplastic binder is studied. Influence of physical condition of binder (powder, film, fiber, granules) on manufacturing technology of prepregs of PCM is shown.

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dx.doi.org/ 10.18577/2307-6046-2015-0-11-6-6

УДК 678.747.2

Platonov A.A., Dushin M.I.

Carbon composites VKU-25 based on unidirectional prepregs

The results of works on development of high-strength polymer composite material of new generation on the basis of a carbon UD fiber and hotmelt resin fulfilled at VIAM are represented in article. Comparative elastic and strength characteristics of the cured composite are submitted. The received results show that the developed carbon composite VKU-25 is not inferior import analogs on is elastic and strength properties .

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dx.doi.org/ 10.18577/2307-6046-2015-0-11-7-7

УДК 678.067.5:614.814.41

Kurnosov A.O., Sokolov I.I., Melnikov D.A., Topunova T.E.

Fireproof fiberglass for interior of passenger aircraft (review)

The article presents information about fiberglass for interior of passenger aircraft developed at VIAM. The basic requirements of fire safety for such materials are pointed out. Methods for determining the combustibility and smoke generation of polymer materials are considered. Main characteristics of fireproof materials based on various types of binders and glass materials are represented. The technology of manufacture of interior panels of different curvature by using the method «crush core» is described.

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Reference list

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12. Zastrogina O.B., Shvets N.I., Postnov V.I., Serkova E.A. Fenolformaldegidnye svjazuyushhie novogo pokoleniya dlya materialov interera [Phenolformaldehyde binding new generation for interior materials] //Aviacionnye materialy i tehnologii. 2012. №S. S. 265–272.
13. Strelnikov S.V., Zastrogina O.B., Veshkin E.A., Shvets N.I. K voprosu o sozdanii vysokoeffektivnyh tehnologij izgotovleniya panelej interera v krupnoserijnom proizvodstve [To a question of creation of highly effective manufacturing techniques of panels of an interior in a large-lot production] //Aviacionnye materialy i tehnologii. 2011. №4. S. 18–24.
14. Serkova E.A., Shvets N.I., Zastrogina O.B., Postnov V.I., Petuhov V.I., Barbotko S.L., Veshkin E.A. Bystrootverzhdaemoe fenolformaldegidnoe svyazujushhee, pererabatyvaemoe po «crush-core» tehnologii, dlya pozharobezopasnyh materialov interera [Quickly cured phenolformaldehyde binding, processed on technology «crush-core», for the fire of safe materials of an interior] /V sb. tezisov dokl. HIH konf. «Konstrukcii i tehnologii poluchenija izdelij iz nemetallicheskih materialov». Obninsk. 2010. S. 70–71.
15. Dolmatovskij M.G., Sokolov I.I. Osobennosti razrusheniya sotovyh panelej so sferoplastikami [Features of destruction of cellular panels with the sphere plasticity] //Aviacionnye materialy i tehnologii. 2008. №4. S. 19–24.

dx.doi.org/ 10.18577/2307-6046-2015-0-11-8-8

УДК 669.715:669.788

Mekhanik E.A., Rastegayeva G.Yu.

Development of the measurement procedure for determination of mass fraction of surface and dissolved hydrogen in aluminum and low aluminum alloys by heating in inert gas argon

Investigation of simultaneous determination of content of surface and dissolved hy-drogen in aluminum and low aluminum alloys was provided by method of heating in an inert gas of argon in electrode impulse furnace of analyzer Leco RHEN-602 followed by detection in the conductivity cell. Operation modes of electrode impulse furnace, allowing complete extraction of surface hydrogen at the first step, and then extraction of dissolved hydrogen from aluminum and low aluminum alloy, were chosen. The measurement procedure was developed using the results of the determination of surface and dissolved hydrogen in different aluminum alloys.

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Reference list

1. Kablov E.N. Osnovnye itogi i napravleniya razvitiya materialov dlya perspektivnoj aviacionnoj tehniki [The main results and the directions of development of materials for the perspective aircraft equipment] /V sb. 75 let. Aviacionnye materialy. Izbrannye trudy «VIAM» 1932–2007: Jubilejnyj nauch.-tehnich. sb. M.: VIAM. 2007. S. 20–26.
2. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative development of FSUE «VIAM» SSC of RF on realization of «Strategic directions of development of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33.
3. Kornysheva I.S., Volkova E.F., Goncharenko E.S., Muhina I.Ju. Perspektivy primeneniya magnievyh i litejnyh alyuminievyh splavov [Prospects of application of magnesian and foundry aluminum alloys] //Aviacionnye materialy i tehnologii. 2012. №S. S. 212–222.
4. Antipov V.V. Strategiya razvitiya titanovyh, magnievyh, berillievyh i alyuminievyh splavov [Strategy of development of titanic, magnesian, beryllium and aluminum alloys] //Aviacionnye materialy i tehnologii. 2012. №S. S. 157–167.
5. Kablov E.N., Ospennikova O.G., Vershkov A.V. Redkie metally i redkozemelnye elementy – materialy sovremennyh i budushhih vysokih tehnologij [Rare metals and rare-earth elements – materials for modern and future high technologies] //Trudy VIAM. 2013. №2. St. 01 (viam-works.ru).
6. Goncharenko E.S., Trapeznikov A.V., Ogorodov D.V. Litejnye alyuminievye splavy (k 100-letiju so dnja rozhdenija M.B. Altmana) [Aluminum casting alloys (on the 100th anniversary of the birth of M. B. Altman)] //Trudy VIAM. 2014. №4. St. 02 (viam-works.ru).
7. Antipov V.V., Senatorova O.G., Tkachenko E.A., Vahromov R.O. Alyuminievye deformiruemye splavy [Aluminum deformable alloys] //Aviacionnye materialy i tehnologii. 2012. №S. S. 167–182.
8. Kablov E.N. Korroziya ili zhizn [Corrosion or life] //Nauka i zhizn. 2012. №11. S. 16–21.
9. Kablov E.N. Aviakosmicheskoe materialivedenie [Aerospace materials science] //Vse materialy. Entsiklopedicheskiy spravochnik. 2008. №3. S. 2–14.
10. Tarasov Yu.M., Antipov V.V. Novye materialy VIAM – dlya perspektivnoj aviacionnoj tehkniki proizvodstva OAO «OAK» [The VIAM new materials – for perspective aviation engineering of production of JSC «OAK»] //Aviacionnye materialy i tehnologii. 2012. №2. S. 5–6.
11. Fridlyander I.N., Grushko O.E., Antipov V.V., Kolobnev N.I., Hokhlatova L.B. Aluminiy-litievye splavy [Aluminum-lithium alloys] /V kn.: 75 let Aviatsionnye materialy. Izbrannye Trudy «VIAM» 1932–2007: Yubileynyi nauch.-tehnich. sb. М.: VIAM. 2007. S. 163–171.
12. Kablov E.N. Sovremennye materialy – osnova innovatsionnoy modernizatsii Rossii [Modern materials – basis of innovative modernization of Russia] //Metally Evrazii. 2012. №3. S. 10–15.
13. Kablov E.N., Lukin V.I., Zhegina I.P., Ioda E.N., Loskutov V.M. Osobennosti I perspektivy svarki alyuminiy-litievyh splavov [Features and perspectives of welding of alyuminiylitiyevy alloys] /V sb. Aviatsionnye materialy i tehnologii. Vyp.: «Tehnologiya proizvodstva aviatsionnyh metallicheskih materilov». M.: VIAM. 2002. S. 3–12.
14. Antipov V.V., Kolobnev N.I., Hohlatova L.B. Razvitie alyuminijlitievyh splavov i mnogostupenchatyh rezhimov termicheskoj obrabotki [Development aluminum lithium alloys and multistage modes of thermal processing] //Aviacionnye materialy i tehnologii. 2012. №S. S. 183–195.
15. Klochkova Ju.Ju., Grushko O.E., Lancova L.P., Burlyaeva I.P., Ovsyannikov B.V. Osvoenie v promyshlennom proizvodstve polufabrikatov iz perspektivnogo aljuminijlitievogo splava V-1469 [Development in industrial production of semi-finished products from perspective alyuminiylitiyevy alloy V-1469] //Aviacionnye materialy i tehnologii. 2011. №1. S. 8–12.

dx.doi.org/ 10.18577/2307-6046-2015-0-11-9-9

УДК 620.1.08:669.018.44:669.245

Karachevtsev F.N., Zagvozdkina T.N., Orlov G.V.

Development and research of metrological characteristics of express-analysis of heat-resistant nickel alloys

Heat-resistant nickel alloys (HRNA) are one of the promising materials, which are used in aviation engineering for manufacture of a wide range of parts and structures for various purposes. Improvement in heat resistance of HRNA depends on the conditions of their production and chemical composition. In this regard control of the composition of HRNA in the process of their production by method of express-analysis is an extremely important problem. The developed method of optical emission analysis provides relative error at determination of the content of alloying elements not more than 5% at values of the mass fraction of more than 1%.

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Reference list

1. Kablov E.N. Fiziko-himicheskie i tehnologicheskie osobennosti sozdaniya zharoprochnyh splavov, soderzhashhih renij [Physical and chemical and technological features of creation of the heat resisting alloys containing rhenium] //Vestnik Moskovskogo universiteta. Ser. 2. Himiya. 2005. T. 46. №3. S. 155–167.
2. Kablov E.N., Lomberg B.S., Ospennikova O.G. Sozdanie sovremennyh zharoprochnyh materialov i tehnologij ih proizvodstva dlya aviacionnogo dvigatelestroeniya [Creation of modern heat resisting materials and technologies of their production for aviation engine-building] //Krylya Rodiny. 2012. №3–4. S. 34–38.
3. Kablov E.N., Ospennikova O.G., Petrushin N.V., Visik E.M. Monokristallicheskij zharoprochnyj nikelevyj splav novogo pokoleniya s nizkoj plotnostyu [Single-crystal nickel-based superalloy of a new generation with low-dencsity] //Aviacionnye materialy i tehnologii. 2015. №2 (35). S. 14–25.
4. Kablov E.N., Petrushin N.V., Svetlov I.L., Demonis I.M. Nikelevye litejnye zharoprochnye splavy novogo pokoleniya [Nickel foundry heat resisting alloys of new generation] //Aviacionnye materialy i tehnologii. 2012. №S. S. 36–52.
5. Lomberg B.S., Ovsepjan S.V., Bakradze M.M., Mazalov I.S. Vysokotemperaturnye zharoprochnye nikelevye splavy dlya detalej gazoturbinnyh dvigatelej [High-temperature heat resisting nickel alloys for details of gas-turbine engines] //Aviacionnye materialy i tehnologii. 2012. №S. S. 52–57.
6. Kablov E.N., Petrushin N.V., Svetlov I.L., Demonis I.M. Litejnye zharoprochnye nikelevye splavy dlya perspektivnyh aviacionnyh GTD [Foundry heat resisting nickel alloys for perspective aviation GTE] //Tehnologiya legkih splavov. 2007. №2. S. 6–16.
7. Shmotin Ju.N., Starkov R.Ju., Danilov D.V., Ospennikova O.G., Lomberg B.S. Novye materialy dlya perspektivnogo dvigatelya OAO «NPO „Saturn”» [New materials for the perspective engine of JSC «NPO „Saturn”»] //Aviacionnye materialy i tehnologii. 2012. №2. S. 6–8.
8. Kablov E.N., Ospennikova O.G., Petrushin N.V. Novyj monokristallicheskij intermetallidnyj (na osnove γʹ-fazy) zharoprochnyj splav dlya lopatok GTD [New single crystal heat-resistant intermetallic γʹ-based alloy for GTE blades] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 34–40.
9. Sidorov V.V., Rigin V.E., Filonova E.V., Timofeeva O.B. Structurnye isslidovaniya i svoistva monokristallov splavov VZhM4-VI i VZhM5-VI [The structure investigations and properties of VGM4-VI and VGM5-VI single crystal alloys with increased phosphorus quantity] // Trudy VIAM. 2014. №3. St. 02. (viam-works.ru).
10. Lomberg B.S., Bakradze M.M., Chabina E.B., Filonova E.V. Vzaimosvjaz struktury i svojstv vysokozharoprochnyh nikelevyh splavov dlya diskov gazoturbinnyh dvigatelej [Interrelation of structure and properties of high-heat resisting nickel alloys for disks of gas-turbine engines] //Aviacionnye materialy i tehnologii. 2011. №2. S. 25–30.
11. Chabina E.B., Filonova E.V., Lomberg B.S., Bakradze M.M. Struktura sovremennyh deformiruemyh nikelevyh splavov [Structure of modern deformable nickel alloys] //Vse materialy. Jenciklopedicheskij spravochnik. 2012. T. 6. S. 22–27.
12. Petrushin N.V., Eljutin E.S., Chabina E.B., Timofeeva O.B. O fazovyh i strukturnyh prevrashhenijah v zharoprochnyh renijsoderzhashhih splavah monokristallicheskogo stroeniya [About phase and structural transformations in heat resisting the reniysoderzhashchikh alloys of a single-crystal structure] //Litejnoe proizvodstvo. 2008. №7. S. 1–7.
13. Letov A.F., Karachevcev F.N., Gundobin N.V., Titov V.I. Razrabotka standartnyh obrazcov sostava splavov aviacionnogo naznacheniya [Development of standard samples of structure of alloys of aviation appointment] //Aviacionnye materialy i tehnologii. 2012. №S. C. 393–398.
14. Letov A.F., Karachevcev F.N. Opyt razrabotki standartnyh obrazcov aviacionnyh splavov [Experience of development of standard samples of aviation alloys] //Mir izmerenij. 2012. №8. S. 31–35.
15. Karachevcev F.N., Letov A.F., Procenko O.M., Jakimova M.S. Razrabotka standartnyh obrazcov sostava aviacionnyh splavov [Development of standard samples of structure of aviation alloys] //Standartnye obrazcy. 2013. №4. S. 30–34.

10.

dx.doi.org/ 10.18577/2307-6046-2015-0-11-10-10

УДК 620.193:669.14.018.8

Belous V.Ya., Loshchinina A.O., Varlamova V.E., Nikitin Ya.Yu.

Corrosion resistance and preparation of a surface of a cold rolled tape from VNS9-Sh steel for production of metalpolymeric composite material

The results of comparative tests of two meltings of cold rolled tape from VNS-9-Sh steel on intergranular corrosion and pitting corrosion are considered in this work. Possibility of preparation of the tape surface by means of etching in various acid solutions in order to manufacture metalpolymeric composite material is investigated. Values of a roughness and influence of etching on plasticity of material are defined.

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11.

dx.doi.org/ 10.18577/2307-6046-2015-0-11-11-11

УДК 621.791.3:543.847

Titov V.I., Goundobin N.V., Pilipenko L.V.

Development of a method for determination of phosphorus in the solder VPr18

In this paper, the possibility for determination of small amounts of phosphorous in the lead-based VPr18 solder used for soldering wires is shown. Small amounts of phosphorous additives can improve corrosion resistance and strength of the material. Thus solder can operate up to temperatures of 270°C. Welding and solder quality depend on the solder composition by major alloying and impurity elements. In this connection it is necessary to clearly regulate the chemical composition of solders and control the content of chemical elements in their composition. A method of determination of small amounts (0,007 wt. %) of phosphorus in the solder VPr18 was developed. When the content of of phosphorus in the the solder material is large it is necessary to build another calibration graph.

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Reference list

1. Rylnikov V.S., Lukin V.I. Pripoi, primenyaemye dlya pajki materialov aviacionnogo naznacheniya [Solders used for soldering materials aviation application] //Trudy VIAM. 2013. №8. St. 02 (viam-works.ru).
2. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative development of FSUE «VIAM» SSC of RF on realization of «Strategic directions of development of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33.
3. Kablov E.N., Mubojadzhjan S.A. Zharostojkie i teplozashhitnye pokrytiya dlya lopatok turbiny vysokogo davleniya perspektivnyh GTD [Heat-resistant and heat-shielding coverings for shovels of the turbine of a high pressure of perspective GTE] //Aviacionnye materialy i tehnologii. 2012. №S. S. 60–70.
4. Kablov E.N., Bondarenko Ju.A., Echin A.B., Surova V.A. Razvitie processa napravlennoj kristallizacii lopatok GTD iz zharoprochnyh splavov s monokristallicheskoj i kompozicionnoj strukturoj [Development of process of the directed crystallization of shovels of GTE of heat resisting alloys with single-crystal and composite structure] //Aviacionnye materialy i tehnologii. 2012. №1. S. 3–8.
5. Kablov E.N., Evgenov A.G., Rylnikov V.S., Afanasev-Hodykin A.N. Issledovanie melkodispersnyh poroshkov pripoev dlya diffuzionnoj vakuumnoj pajki, poluchennyh metodom atomizacii rasplava [Research of fine powders of the solders for the diffusive vacuum soldering received by a fusion atomization method] //Vestnik MGTU im. N.Je. Baumana. Ser. «Mashinostroenie». 2011. №SP2. S. 79–87.
6. Sorokin L.I. Svarivaemost zharoprochnyh splavov, primenjaemyh v aviacionnyh gazoturbinnyh dvigatelyah [The weldability of the heat resisting alloys applied in aviation gas-turbine engines] //Svarochnoe proizvodstvo. 1997. №4. S. 4–11.
7. Lukin V.I., Semenov V.N., Starova L.L. i dr. Obrazovanie gorjachih treshhin pri svarke zharoprochnyh splavov [Formation of hot cracks when welding heat resisting alloys] //MiTOM. 2007. №12. S. 7–14.
8. Rylnikov V.S. Voprosy po pajke, reshennye v processe izgotovleniya izdeliya «Buran» [Some problems of brazing solved in the course of manufacture of «Buran» reusable spaceship] //Aviacionnye materialy i tehnologii. 2013. №S1. S. 33–34.
9. Lukin V.I., Banas I.P., Kovalchuk V.G., Golev E.V. Argono-dugovaja svarka vysokoprochnoj cementuemoj stali VNS-63 [TIG welding of high-strengthened cemented steel VNS-63] //Trudy VIAM. 2013. №8. St. 01 (viam-works.ru).
10. Afanasev-Hodykin A.N., Lukin V.I., Rylnikov V.S. Vysokotehnologichnye polufabrikaty zharoprochnyh pripoev (lenty i pasty na organicheskom svyazujushhem) [Hi-tech semi-finished high-temperature solders (tape and paste on an organic)] //Trudy VIAM. 2013. №9. St. 02 (viam-works.ru).
11. Rylnikov V.S., Afanasev-Hodykin A.N., Galushka I.A. Tehnologiya pajki konstrukcii tipa «blisk» iz raznoimennyh splavov [Technology of braze design type «blisk» from dissimilar alloys] //Trudy VIAM. 2013. №10. St. 02 (viam-works.ru).
12. Rylnikov V.S., Afanasev-Hodykin A.N., Krasikov M.I. Issledovanie remontnoj tehnologii ispravleniya defektov pajanyh soedinenij toplivnyh kollektorov [Research of repair technology of defects correction of soldered joints of fuel collector] //Trudy VIAM. 2013. №12. St. 02 (viam-works.ru).
13. Khorunov V.F., Maksimova S.V. Paika zharoprochnykh splavov na sovremennom etape [The soldering of hot strength alloys at the present stage] //Svarochnoe proizvodstvo. 2010. №10. S. 24–27.
14. Lukin V.I., Banas I.P., Kovalchuk V.G., Golev E.V. Argono-dugovaya svarka visokoprochnoi cementuemoy staly VNS-63 [Argon-arc welding of high-strength VNS-63 cemetey steel] // Trudy VIAM. 2013. №8. St. 01 (viam-works.ru).
15. Krivusha L.S., Sukhomlin M.M., Vorobev G.M. Problema kachestva payanykh soedineniy I razrabotka pripoev [Problem of quality of sweated connections and development of solders] //Avtomatocheskaya svarka. 2005. №3. S. 48–53.

12.

dx.doi.org/ 10.18577/2307-6046-2015-0-11-12-12

УДК 543.5:546.76

Alekseev A.V., Yakimovitch P.V.

Microwave sample preparation of chrome for determination of contaminants by method of IСP-MS

The technique of microwave sample preparation of chrome for determination of a mass fraction of Si, P, Fe, Cu, Zn, As, Sn, Sb, Pb and Bi by mass spectrometry with inductively coupled plasma method (IСP-MS) is described, and also test for content of these elements in a chrome sample is carried out. Compositions of mixes for dissolution, an order of addition of reagents and parameters of microwave decomposition are chosen. Spectral interferences are eliminated by means of reaction-collision cell application. The correctness of measurement techniques is verified by the «added–found» method. Range of the determination contents made 0,00001–0,18 mass %.

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Reference list

1. Reformatskaya I.I., Podobaev A.N., Shilov D.S., Chibysheva D.V., Artamonov O.Ju. Rol hroma v korrozionno-elektrohimicheskom povedenii uglerodistyh stalej [Chrome role in corrosion and electrochemical behavior carbonaceous the steel] //Izvestija MGTU «MAMI». 2013. T. 4. №1. S. 89–96.
2. Kolokolcev V.M., Golcov A.S., Stolyarov A.M. Vybor novogo sostava zharoiznosostojkogo chuguna [Choice of new composition of heat and wear resistant cast iron] //Litejnoe proizvodstvo. 2013. №6. S. 2–7.
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4. Splav dlya izgotovleniya shtampovogo instrumenta [Alloy for production of the stamp tools]: pat. 2392341 Ros. Federaciya; opubl. 20.06.10.
5. Amirhanova N.A., Hamzina A.R. Povyshenie korrozionnoj stojkosti splava JeP648k vysokotemperaturnoj gazovoj korrozii [Increase of corrosion resistance of alloy EP648k of high-temperature gas corrosion] //Vestnik PNIPU. Aerokosmicheskaya tehnika. 2014. №36.
S. 38–48.
6. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33.
7. Kablov E.N., Ospennikova O.G., Vershkov A.V. Redkie metally i redkozemelnye elementy – materialy sovremennyh i budushhih vysokih tehnologij [Rare metals and rare-earth elements – materials for modern and future high technologies] //Trudy VIAM. 2013. №2. St. 01 (viam-works.ru).
8. Min P.G., Sidorov V.V. Opyt pererabotki litejnyh othodov splava ZhS32-VI na nauchno-proizvodstvennom komplekse FGUP «VIAM» po izgotovleniyu lityh prutkovyh (shihtovyh) zagotovok [The experience of GS32-VI alloy scrap recycling at the VIAM scientific and production complex for cast bars production] //Aviacionnye materialy i tehnologii. 2013. №4. S. 20–25.
9. Kablov E.N., Bondarenko Ju.A., Echin A.B., Surova V.A. Razvitie processa napravlennoj kristallizacii lopatok GTD iz zharoprochnyh splavov s monokristallicheskoj i kompozicionnoj strukturoj [Development of process of the directed crystallization of shovels of GTE of heat resisting alloys with single-crystal and composite structure] //Aviacionnye materialy i tehnologii. 2012. №1. S. 3–8.
10. Min P.G., Sidorov V.V. Rafinirovanie othodov zharoprochnogo nikelevogo splava ZhS32-VI ot primesi kremniya v usloviyah vakuumnoj indukcionnoj plavki [Refining of scrap of Ni-base superalloy GS32-VI to eliminate silicon impurity under conditions of vacuum induction melting] //Trudy VIAM. 2014. №9. St. 01 (viam-works.ru).
11. Kablov E.N., Lomberg B.S., Ospennikova O.G. Sozdanie sovremennyh zharoprochnyh materialov i tehnologij ih proizvodstva dlja aviacionnogo dvigatelestroenija [Creation of modern heat resisting materials and technologies of their production for aviation engine-building] //Krylja Rodiny. 2012. №3–4. S. 34–38.
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14. MI 1.2.052–2013. Metodika izmerenij massovoj doli primesej Р, Mn, Fe, Cu, Zn, Ga, As, Se, Ag, Cd, Sn, Sb, Te, Tl, Pb, Bi v nikelevyh splavah metodom mass-spektrometrii s induktivno svyazannoj plazmoj [Measurement technique of a mass fraction of impurity Р, Mn, Fe, Cu, Zn, Ga, As, Se, Ag, Cd, Sn, Sb, Te, Tl, Pb, Bi in nickel alloys by a mass spectrometry method with inductively connected plasma].
15. Pupyshev A.A., Surikov V.T. Mass-spektrometriya s induktivno svjazannoj plazmoj. Obrazovanie ionov [Mass spectrometry with inductively connected plasma. Formation of ions]. Ekaterinburg: UrO RAN. 2006. 276 s.
16. Tormysheva E.A., Smirnova E.V., Ermolaeva T.N. Opredeleniya oksidov zheleza (III), kalciya i alyuminiya v magnezialnyh ogneuporah metodom AJeS s ISP v usloviyah mikrovolnovogo razlozheniya proby [Definitions of oxides of iron (III), calcium and aluminum in magnesian refractory materials by method of the NPP with ISP in the conditions of microwave decomposition of test] //Vestnik Voronezhskogo gosudarstvennogo universiteta. 2010. №1. S. 51–55