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dx.doi.org/ 10.18577/2307-6046-2017-0-9-1-1

УДК 669.295

Nochovnaya N.A., Panin P.V.

Phase composition and structure formation in VT5, VT20, and VT6 titanium alloys upon thermo-hydrogen treatment and plastic deformation

A complex approach to structure and properties transformation of titanium alloys has been in focus, the approach including thermo-hydrogen treatment and plastic deformation combination. It has been shown that thermo-hydrogen treatment together with plastic deformation allow to obtain a multiphase structure in 2 mm sheet semi-finished products of VT5 (Ti–5,8Al), VT20 (Ti–6,2Al–1,2V–1Mo–2Zr), and VT6 (Ti–5,7Al–4,3V) titanium alloys (wt.%). The obtained structure contain α-phase in two structural constituents: primary αI-phase enriched by aluminum up to Ti3Al-based α2-phase, and secondary αdeg-phase depleted by aluminum.

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Reference list

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16. Skvorcova S.V., Popova Ju.A., Panin P.V., Grushin I.A., Kuryshev E.A. Vlijanie termicheskoj obrabotki na strukturu i svojstva svarnyh soedinenij iz titanovogo splava VT23 [Influence of thermal processing on structure and property of welded connections from BT23 titanium alloy] // Titan. 2011. №2 (32). S. 16–21.
17. Skvorcova S.V., Panin P.V., Nochovnaja N.A., Grushin I.A., Mitropolskaja N.G. Vlijanie vodoroda na fazovye i strukturnye prevrashhenija v titanovom splave VT6 [Influence of hydrogen on phase and structural transformations in BT6 titanium alloy] // Tehnologija legkih splavov. 2011. №4. S. 35–40.
18. Panin P.V., Dzunovich D.A., Zasypkin V.V. Sozdanie dvuhfaznoj kompozitnoj struktury v alfa-splave Ti–6Al s pomoshhju termovodorodnoj obrabotki [Creation of diphasic composite structure in Ti–6Al alpha alloy by means of thermohydrogen treating] // Nauchnye trudy (Vestnik MATI). 2012. №19 (91). S. 33–37.
19. Panin P.V., Grushin I.A., Mitropol'skaja N.G. Issledovanie zakonomernostej izmenenija strukturno-fazovogo sostojanija titanovogo splava VT6 pri dopolnitelnom legirovanii vodorodom [Research of patterns of change of structural and phase condition of BT6 titanium alloy at additional alloying hydrogen] // Nauchnye trudy (Vestnik MATI). 2013. №20 (92). S. 31–34.
20. Panin P.V., Shirjaev A.A., Dzunovich D.A. Postroenie temperaturno-koncentracionnoj diagrammy fazovogo sostava titanovogo splava VT6, dopolnitel'no legirovannogo vodorodom [Creation of the temperature and concentration chart of phase composition of the BT6 titanium alloy which has been in addition alloyed by hydrogen] // Tehnologija mashinostroenija. 2014. №3 (141). S. 5–9.
21. Panin P.V., Dzunovich D.A., Alekseev E.B. Sposoby opisaniya fazovogo sostava titanovyh splavov, dopolnitelno legirovannyh vodorodom (obzor) [Ways of phase areas representation in titanium alloys additionally doped with hydrogen (review)] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2015. №3. St. 03. Available at: http://www.viam-works.ru (accessed: August 07, 2017). DOI: 10.18577/2307-6046-2015-0-3-3-3.
22. Panin P.V., Dzunovich D.A., Alekseev E.B. Fazovyj sostav i struktura titanovogo splava VT6, dopolnitelno legirovannogo vodorodom, posle vakuumnogo otzhiga [Phase composition and structure of hydrogenated titanium alloy VT6 after vacuum annealing] // Trudy VIAM: jelektron. nauch.-tehnich. zhurn. 2016. №2 (38). St. 05. Available at: http://www.viam-works.ru (accessed: August 07, 2017). DOI: 10.18577/2307-6046-2016-0-2-5-5.
23. Panin P.V., Dzunovich D.A., Shiryaev A.A. Issledovanie termicheskoj stabilnosti struktury titanovogo splava VT6 posle termovodorodnoj obrabotki [Research on thermal stability of VT6 titanium alloy structure after thermohydrogen treatment] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2016. №3. St. 06. Available at: http://www.viam-works.ru (accessed: August 07, 2017). DOI: 10.18577/2307-6046-2016-0-3-6-6.
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27. Kablov D.E., Panin P.V., Shiryaev A.A., Nochovnaya N.A. Opyt ispolzovaniya vakuumno-dugovoj pechi ALD VAR L200 dlya vyplavki slitkov zharoprochnyh splavov na osnove alju-minidov titana [The use of ADL VAR L200 vacuum-arc furnace for ingots fabrication of high-temperature titanium aluminides base alloys] //Aviacionnye materialy i tehnologii. 2014. №2 (31). S. 27–33. DOI: 10.18577/2071-9140-2014-0-2-27-33.
28. Ilin A.A. Mehanizm i kinetika fazovyh i strukturnyh prevrashhenij v titanovyh splavah [The mechanism and kinetics of phase and structural transformations in titanium alloys]. M.: Nauka, 1994. 304 s.

dx.doi.org/ 10.18577/2307-6046-2017-0-9-2-2

УДК 669.295

Nochovnaya N.A., Shiryaev A.A.

FSUE «VIAM» experience in strips production of a new high-strength metastable β-titanium alloy VT47

Both technological process protocol and parameters have been developed for a high-strength metastable -titanium REE-containing VT47 alloy, and pilot samples of strips have been produced thereof. The effect of temperature and rate parameters upon interoperation heat treatment (quenching) on mechanical properties of the strips has been studied. A complex quality evaluation of the pilot strips samples, including research on structure and mechanical properties, has showed a reasonability of further work on optimization of strips and foils production technologies for VT47 alloy.

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Reference list

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dx.doi.org/ 10.18577/2307-6046-2017-0-9-3-3

УДК 66.017:623.4

Eliseev E.A., Tonysheva О.А., Yakusheva N.A.

Materials and development of the technologies providing the resource trunks of artillery, tank and shooting systems of arms (review)

Barrel of different guns and small arms are training in different atmospheric and weather conditions by the contingent of different degree of readiness. Different materials and various technologies of their processing are used for barrels manufacturing. There are identical and specific requirements to barrels which are differ from each other depending on fighting assignment of tools, installation on vehicle and caliber. A trunk is most loaded detail of the weapon and its resource is considerably smaller than all other nodes and details of a weapon. The factors influencing weapon trunks, materials for manufacturing of trunks and ways of their processing are considered in the article.

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Reference list

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25. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] // Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.

dx.doi.org/ 10.18577/2307-6046-2017-0-9-4-4

УДК 621.762:669.046.516.2

Buyakina A.A., Letnikov M.N., Efimochkin I.Yu.

The influence of the mechanical alloying parameters on the particles morphology of the metalceramiс powder composition made from VZH175 alloy with TiCN nanopowder

The influence of the main parameters of the mechanical alloying in the planetary ball mill on flowability and morphology of the metalceramiс made from Ni-based superalloy VGH175 and nanoparticles of titanium carbonitride are investigated. As the basis of metalceramiс composition have been used powder of VGH175 superalloy with particle size less than 63 μm produced by gas atomization; аs the reinforcing filler have been used nanoparticles of titanium carbonitride produced by the plasma-chemical synthesis method. The effect of the rotation speed of grinding jars and time process on flowability of compositions and morphology of the particles (average diameter and powder-size distribution) are presented. The optimal parameters for producing metalceramiс powders with the uniform distribution of the nanoparticles on the matrix granules surface with keepping their original spherical form are determined.

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1. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the develop-ment of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
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4. Kablov E.N., Ospennikova O.G., Lomberg B.S. Kompleksnaya innovacionnaya tehnologiya izotermicheskoj shtampovki na vozduhe v rezhime sverhplastichnosti diskov iz superzharoprochnyh splavov [Complex innovative technology of isothermal punching on air in mode of superplasticity of disks from superhot strength alloys] // Aviacionnye materialy i tehnologii. 2012. №S. S. 129–141.
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16. Samohin A.V., Alekseev N.V., Sinajskij M.A., Cvetkov Ju.V. Ravnovesnye jenergotehnologicheskie harakteristiki plazmennyh processov poluchenija nitrida, karbida i karbonitrida titana iz hlorida titana [Equilibrium power technical characteristics on plasma processes of receiving nitride, carbide and carbotitanium nitride from titanium chloride] // Fizika i himija obrabotki materialov. 2015. №4. S. 18–24.

dx.doi.org/ 10.18577/2307-6046-2017-0-9-5-5

УДК 678.073

Sorokin A.E., Platonov M.M., Larionov S.A.

Selective laser sintering of polymer compositions based on polyamide 12

Studies of crystallization from solution and processing by selective laser alloying of polyamide 12 based compositions have been carried out. It has been shown that process of crystallization under conditions close to equilibrium in the presence of nanoscale silicon dioxide makes it possible to obtain powder compositions with an optimal complex of properties. It has been found that Powder compositions with a narrow particle size distribution (from 20 to 100 μm) and a bulk density of not less than 0,4 g/cm3 can be processed by selective laser sintering into homogeneous samples with a high degree of monolithicity.

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Reference list

1. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the develop-ment of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
2. Kablov E.N. Materialy i khimicheskie tekhnologii dlya aviatsionnoy tekhniki [Materials and chemical technologies for aviation engineering] // Vestnik Rossiyskoy akademii nauk. 2012. T. 82. №6. S. 520–530.
3. Kablov E.N. Aviakosmicheskoe materialovedenie [Aerospace materials science] // Vse materialy. Entsiklopedicheskiy spravochnik. 2008. №3. S. 2–14.
4. Kablov E.N. Tendentsii i orientiry innovatsionnogo razvitiya Rossii [Tendencies and reference points of innovative development of Russia]: sb. nauch.-inform. mater. 3-e izd. M.: VIAM, 2015. 720 s.
5. Petrova G.N., Rumyanceva T.V., Beyder E.Ya. Vliyanie modificiruyushhih dobavok na pozharobezopasnye svojstva i tehnologichnost polikarbonata [Influence of modifying additives on fireproof properties and technological effectiveness of polycarbonate] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2013. №6. St. 06. Available at: http://www.viam-works.ru (accessed: July 25, 2016).
6. Barbotko S.L. Pozharobezopasnost aviacionnyh materialov [Fire safety of aviation materials] // Aviacionnye materialy i tehnologii. 2012. №S. S. 431–439.
7. Platonov M.M., Larionov S.A. Issledovanie fazovyh perehodov i struktury polimernyh poroshkovyh kompozicij na osnove polidodekalaktama, poluchennyh metodom kristallizacii iz rastvorov v poljarnyh aprotonnyh rastvoriteljah [Investigation of phase transitions and structure of the polymer powder compositions based on polydodecanolactam obtained by crystallization from solutions in polar aprotic solvents] // Aviacionnye materialy i tehnologii. 2016. №S1 (43). S. 65–73. DOI: 10.18577/2071-9140-2016-0-S1-65-73.
8. Huang S.H., Liu P., Mokasdar A., Hou L. Additive manufacturing and its societal impact: a literature review // Int. J. Adv. Manuf. Technol. 2013. Vol. 67. P. 1191–1203. DOI: 10.1007/s00170-012-4558-5.
9. Bikas H., Stavropoulos P., Chryssolouris G. Additive manufacturing methods and modeling approaches: a critical review // Int. J. Adv. Manuf. Technol. 2016. Vol. 83. P. 389–405. DOI: 10.1007/s00170-015-7576-2.
10. Novakova-Marcincinova L., Kuric I. Basic and Advanced Materials for Fused Deposition Modeling Rapid Prototyping Technology // Manuf. and Ind. Eng. 2012. Vol. 11 (1). P. 24–27.
11. Hill N., Haghi M. Deposition direction-dependent failure criteria for fused deposition modeling polycarbonate // Rapid Prototyping Journal. 2014. Vol. 20/3. P. 221–227. DOI: 10.1108/RPJ-04-2013-0039.
12. Goodridge R.D., Tuck C.J., Hague R.J.M. Laser sintering of polyamides and other polymers // Progress in Materials Science. 2012. Vol. 57. P. 229–267. DOI: 10.1016/j.pmatsci.2011.04.001.
13. Kruth J.-P., Levy G., Klocke F., Childs T.H.C. Consolidation phenomena in laser and powder-bed based layered manufacturing // Annals of the CIRP. 2007. Vol. 56/2. P. 730–759. DOI: 10.1016/j.cirp.2007.10.004
14. Process for the manufacture of polyamide 12 powder with a high melting point: pat. CA 2498712 C; publ. 15.06.10.
15. Use of a polyamide 12 for selective laser sintering: pat. EP 0911142 B1; publ. 03.08.05.
16. Method of selective laser sintering with improved materials: pat. US 7794647 B1; publ. 14.08.06.
17. Seltzera R., De la Escalerab F.M., Seguradoa J. Effect of water conditioning on the fracture behavior of PA12 composites processed by selective laser sintering // Materials Science and Engineering A. 2011. Vol. 528. P. 6927–6933. DOI: 10.1016/j.msea.2011.05.045.
18. Schmid M., Amado A., Wegener K. Polymer Powders for Selective Laser Sintering (SLS) // 30th International Conference of the Polymer Processing Society. Cleveland, Ohio, 2014. P. 7–12.
19. Tager A.A. Fiziko-himija polimerov [Fiziko-himiya polymers]. 4-e izd., pererab. i dop. M.: Nauchnyj mir. 2007. 573 s.
20. Harakteristiki poroshkovoj kompozicii RA 2200 [Characteristics of powder composition of PA 2200] // e-Manufacturing solutions: katalog materialov kompanii EOS. Available at: http://eos.materialdatacenter.com/eo/ (accessed: July 26, 2017).
21. Harakteristiki poroshkovoj kompozicii PA-12 AdSint [Characteristics of powder composition of PA-12 AdSint] // Material for additive manufacturing: katalog materialov kompanii ADVANC3D Materials® GmbH. Available at: http://www.advanc3dmaterials.com/assets/presentation-sls.pdf (accessed: July 26, 2017).
22. Harakteristiki poroshkovoj kompozicii FS3200PA [Characteristics of powder composition of FS3200PA] // Farsoon technologies: katalog materialov kompanii Human Farsoon High-tech Co. Ltd. Available at: http://www.farsoon.us/wp-content/uploads/2015/04/3200PA_Specs.pdf (accessed: July 26, 2017).

dx.doi.org/ 10.18577/2307-6046-2017-0-9-6-6

УДК 678.073

Petrova G.N., Starostina I.V., Rumyantseva T.V., Sapego Yu. A.

Efficiency of improvement of quality of products from polycarbonate heat treatment

Results of researches on influence of modes of heat treatment of polycarbonate are given in article on quality of products made of it, Is shown that the choice of thermoplastic is caused by high level of the physicist – mechanical properties, dimensional stability, high accuracy when molding, good decorative look, and also expansion of areas of its application. Conditions of need of carrying out heat treatment for this material are given. It is shown that simple on configuration, thin-walled, irresponsible assignment of detail can be not subjected to heat treatment; at the same time the details working in the field of high temperatures, in surface-active environments, details of difficult configuration and having metal armature, it is reasonable to subject to heat treatment. Results of influence of different modes of heat treatment (tempering, annealing, etc.) on physical, strength and deformation properties of samples of material are given. On the basis of the received test results

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Reference list

1. Sadova A.N., Kuznecova O.N., Arhireev V.P. i dr. Principy upravleniya kachestvom polimernoj produkcii [Principles of quality management of polymeric products]. M.: KolosS, 2009. 319 s.
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5. Sudarushkin Yu.K., Gudimov M.M., Romanov D.S., Sokolov M.Yu. Primenenie litevyh polikarbonatov v aviapriborostroenii [Application of molding polycarbonates in avionics] // Aviacionnaya promyshlennost. 2003. №2. S. 48–52.
6. Petrova G.N., Bejder E.Ya., Starostina I.V. Litevye termoplasty dlya izdelij aviacionnoj tehniki [Molding thermoplastics for products of aviation engineering] // Vse materialy. Enciklopedicheskij spravochnik. 2016. №6. S. 10–15.
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16. Petrova G.N., Larionov S.A., Platonov M.M., Perfilova D.N. Termoplastichnye materialy novogo pokoleniya dlya aviacii [Thermoplastic materials of new generation for aviation] // Aviacionnye materialy i tehnologii 2017. №S. S. 420–436. DOI: 10.18577/2071-9140-2017-0-S-420-436.
17. Petrova G.N., Platonov M.M., Bolshakov V.A., Ponomarenko S.A. Issledovanie kompleksa harakteristik bazovyh materialov dlya FDM tehnologii additivnogo sinteza. Fiziko-mehanicheskie i teplofizicheskie svojstva [Research of complex of characteristics of base materials for FDM technology of the additive synthesis. Physicomechanical and heatphysical properties] // Plasticheskie massy. 2016. №5–6. S. 53–58.
18. Petrova G.N., Larionov S.A., Sapego Yu.A., Platonov M.M. Reologicheskie svojstva termoplastichnoj kompozicii na osnove polikarbonata: zavisimost ot temperatury pererabotki; vliyanie na mehanicheskie harakteristiki i razmernuyu stabilnost obektov, sozdannyh po FDM-tehnologii [Rheological properties of the thermoplastic composition with a reduced fire hazard polycarbonate-based: depending on the temperature processing; effect on mechanical properties and stability dimension objects created software FDM-technology] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2017. №4 (52). St. 09. Available at: http://viam-works.ru (accessed: July 19, 2017). DOI: 10.18577/2307-6046-2017-0-4-9-9.
19. Platonov M.M., Petrova G.N., Larionov S.A., Barbotko S.L. Optimizaciya sostava polimernoj kompozicii s ponizhennoj pozharnoj opasnostyu na osnove polikarbonata dlya tehnologii 3D-pechati rasplavlennoj polimernoj nityu [Optimization of structure of polymeric composition with the lowered fire danger on the basis of polycarbonate for technology of the 3D-press the melted polymeric thread] // Izvestiya vuzov. Himiya i himicheskaya tehnologiya. 2017. T. 60. №1. S. 87–94.
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26. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] // Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.

dx.doi.org/ 10.18577/2307-6046-2017-0-9-7-7

УДК 699.81:678.073

Petrova G.N., Sapego Yu. A., Larionov S.A., Platonov M.M., Laptev A.B.

Fireproof thermoplastic materials for 3D-technologies

Results of researches of the fireproof thermoplastic materials developed in VIAM Federal State Unitary Enterprise for use in FDM of the additive technology 3D are given in article – the press. Requirements for level of utilization and technical characteristics to which such materials have to answer are formulated. Physical-mechanical, rheological and fireproof properties of the developed thermoplastic compositions on the basis of polycarbonate and polyamide are considered. Test results of the samples received on traditional casting technology under pressure and innovative way 3D – the press are given. It is shown that the developed materials on level of properties and technological effectiveness do not concede to foreign analogs. The interrelation between technological parameters of level-by-level synthesis of object (temperature of extrusion, camera temperature, orientation of molecules in strand) on the accuracy of the press and its strength properties is defined. The received pat

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Reference list

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3. Kablov E.N., Semenova L.V., Petrova G.N., Larionov S.A., Perfilova D.N. Polimernye kompozicionnye materialy na termoplastichnoj matrice [Polymeric composite materials on thermoflexible matrix] // Izvestiya vuzov. Ser.: Himiya i himicheskaya tehnologiya. 2016. T. 59. №10. S. 61–71.
4. Kablov E.N. Aviakosmicheskoe materialovedenie [Aerospace materials science] // Vse materialy. Enciklopedicheskij spravochnik. 2008. №3. S. 2–14.
5. Sudarushkin Yu.K., Gudimov M.M., Romanov D.S., Sokolov M.Yu. Primenenie lit'evyh polikarbonatov v aviapriborostroenii [Application of lityevy polycarbonates in avionics] // Aviacionnaya promyshlennost. 2003. №2. S. 48–52.
6. Petrova G.N.. Bejder E.Ya., Starostina I.V. Molding termoplasty dlya izdelij aviacionnoj tehniki [Lityevye thermoplastics for products of aviation engineering] // Vse materialy. Enciklopedicheskij spravochnik. 2016. №6. S. 10–15.
7. Kerber M.L., Vinogradov V.M., Golovkin G.S. i dr. Polimernye kompozicionnye materialy: struktura, svojstva, tehnologiya [Polymeric composite materials: structure, properties, technology]. SPb.: Professiya, 2011. S. 32–33.
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12. Sorokin A.E., Bejder E.Ya., Perfilova D.N. Vliyanie klimaticheskih faktorov na svojstva ugleplastika na polifenilensulfidnom svyazuyushhem [Effect of climatic factors on properties of carbon fiber reinforced plastic based on polyphenylenesulfide resin] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2015. №1. St. 10. Available at: http://www.viam-works.ru (accessed: July 12, 2017). DOI: 10.18577/2307-6046-2015-0-1-10-10.
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14. Nazarov V.G., Stolyarov V.P., Petrova G.N., Gryaznov V.I., Buznik V.M. Osobennosti poverhnostnogo ftorirovaniya termoelastoplastov na osnove poliuretana i ego vliyanie na svojstva polimera [Features of surfacing fluorine of thermoelastoplastics on the basis of polyurethane and its influence on properties of polymer] // Perspektivnye materialy. 2016. №2. S. 52–60.
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16. Sorokin A.E., Krasnov A.P., Zyuzina G.F. i dr. Stroenie i svojstva vysokomolekulyarnogo lit'evogo poliarilata [Structure and properties of high-molecular molding polyarylate] // Plasticheskie massy. 2012. №1. S. 8–12.
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18. Kondrashov S.V., Shashkeev K.A., Petrova G.N., Mekalina I.V. Polimernye kompozicionnye materialy konstrukcionnogo naznacheniya s funkcionalnymi svojstvami [Constructional polymer composites with functional properties] // Aviacionnye materialy i tehnologii. 2017. №S. S. 405–419. DOI: 10.18577/2071-9140-2017-0-S-405-419.
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35. Platonov M.M., Petrova G.N., Larionov S.A., Barbotko S.L. Optimizaciya sostava polimernoj kompozicii s ponizhennoj pozharnoj opasnostyu na osnove polikarbonata dlya tehnologii 3D-pechati rasplavlennoj polimernoj nityu [Optimization of structure of polymeric composition with the lowered fire danger on the basis of polycarbonate for technology of the 3D-press the melted polymeric thread] // Izvestiya vuzov. Himiya i himicheskaya tehnologiya. 2017. T. 60. №1. S. 87–94.
36. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] // Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.

dx.doi.org/ 10.18577/2307-6046-2017-0-9-8-8

УДК 620.179

Beljaev А.А., Bespalova E.E., Payarel S.M.

Features of measurement of dielectric characteristics by means of the slot-hole resonator

In aviation and space technology are widely used materials to ensure absorption or passage of electromagnetic energy – radioabsorbing (RAM) and radio-transparent materials. When designing RРM, especially multi-layer broadband and very important point is determined experimentally of the reflection coefficient (RC) dielectric and magnetic properties of the individual layers of material in a given frequency range (from UHF to millimeter wavelengths). One of the simplest methods for measuring dielectric and magnetic properties of materials is a waveguide method. However, measurements of permeability measurement in waveguides are inherent in large errors due to the inaccu-racy of sample preparation. In addition, at frequencies above 10 GHz waveguide section dimensions become smaller inhomogeneously stey heterogeneous materials, which does not allow for measurement at these frequencies. The measurements were carried out only at certain points range and extremely time-consuming. Resonator m

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Reference list

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5. Kablov E.N. Konstrukcionnye i funkcionalnye materialy – osnova ekonomicheskogo i nauchno-tehnicheskogo razvitiya Rossii [Constructional and functional materials are the base of economic and scientific and technical development of Russia] // Voprosy materialovedeniya. 2006. №1. S. 64–67.
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9. Lushina M.V., Parshin S.G., Rzhevskij A.A. Sovremennye ekraniruyushhie i radiopogloshhayushhie materialy [Modern shielding and radio absorbing materials] // Sistemy upravleniya i obrabotka informacii. 2011. №22. S. 208–223.
10. Bibikov S.B., Titov A.N., Cherepanov A.K. Sintez materiala s zadannym koefficientom otrazheniya v shirokom diapazone chastot i uglov padeniya [Material synthesis with the set reflection coefficient with the broad range of frequencies and incidence angles] // Sb. dokl. XV Mezhdunar. nauch.-tehnich. konf. «Radiolokaciya. Navigaciya. Svyaz». Voronezh, 2009. S. 1578–1584.
11. Mishhenko S.V., Malkov N.A. Proektirovanie radiovolnovyh (SVCh) priborov nerazrushayushhego kontrolya materialov: ucheb. posobie [Design of radio wave (microwave ovens) of devices of non-destructive testing of materials]. Tambov: Izd-vo TGU, 2003. 128 s.
12. Bannyj V.A., Carenko I.V. Radiopogloshhayushhie materialy na osnove napolnennogo polietilena [Radio absorbing materials on the basis of the filled polyethylene] // Vestnik GGTU im. P.O. Suhogo. 2009. №4. S. 3–8.
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15. Garin B.M., Dyakonova O.A., Kazancev Yu.N. Fizicheskie svojstva rezistivnyh nitej i struktur na ih osnove v SVCh diapazone [Physical properties of resistive threads and structures on their basis in the microwave oven range] // Zhurnal tehnicheskoj fiziki. 1999. T. 69. Vyp. 1. S. 104–108.
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18. Bespalova E.E., Belyaev A.A., Romanov A.M., Shirokov V.V. Issledovanie dielektricheskih harakteristik sloev mnogoslojnogo radiopogloshhayushhego materiala dlya bezehovyh kamer na osnove vspenennogo asbesta, napolnennogo nauglerozhennym voloknom [Investigation of the dielectric characteristics of designed for anechoic chambers laminated radar absorbing material layers based with carbonized fiber filled foam asbestos] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2014. №8. St. 12. Available at: http://www.viam-works.ru (accessed: July 15, 2017). DOI: 10.18577/2307-6046-2014-0-8-12-12.
19. Brandt L.A. Issledovaniya dielektrikov na sverhvysokih chastotah [Researches of dielectrics at super-high frequencies]. M.: Gos. izd-vo fiz.-mat. lit., 1963. S. 191–201.
20. Shirokov V.V., Romanov A.M. Issledovanie dielektricheskih harakteristik steklosotoplasta volnovodnym metodom [Waveguide method research of honeycomb glass fibre plastics dielectric characteristics] // Aviacionnye materialy i tehnologii. 2013. №4. S. 62–68.
21. Belyaev A.A., Romanov A.M., Shirokov V.V., Shuldeshov E.M. Izmerenie dielektricheskoj pronicaemosti steklosotoplasta v svobodnom prostranstve [Measurement of honeycomb glass fiber plasticspermittivity in free space] // Trudy VIAM: elektron. nauch-tehnih. zhurn. 2014. №5. St. 06. Available at: http://viam-works.ru (accessed: July 19, 2017). DOI: 10.18577/2307-6046-2014-0-5-6-6.
22. Romanov A.M., Belyaev A.A., Bespalova E.E. Nedostatki volnovodnyh metodov izmereniya harakteristik radiopogloshhayushhih materialov [Disadvantages of waveguide techniques for measurement of radar-absorbing material characteristics] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2015. №3. St. 11. Available at: http://www.viam-works.ru (accessed: July 19, 2017). DOI: 10.18577/2307-6046-2015-0-3-11-11.
23. Kolosov Yu.A., Levkov F.E. Tochnostnye harakteristiki volnovodnogo metoda opredeleniya elektricheskih parametrov dielektrikov [Precision characteristics of the waveguide method of determination of electric parameters of dielectrics] // Voprosy radioelektroniki. Ser.: Obshhie voprosy radioelektroniki. 1985. №12. S. 18–33.
24. Kolosov Yu.A., Levkov F.E. O volnovodnom metode opredeleniya elektricheskih parametrov dielektrikov [About the waveguide method of determination of electric parameters of dielectrics] // Voprosy radioelektroniki. Ser.: Obshhie voprosy radioelektroniki. 1986. №1. S. 41–45.

dx.doi.org/ 10.18577/2307-6046-2017-0-9-9-9

УДК 665.939.5

Petrova A.P., Isaev A.Yu.

Thermal stability of carborane-containing adhesive systems

The effect on the thermal stability of adhesive systems on the basis of various types of polymers (phenolrubber, organosilicon, polyurethane, organo-organic) their modification with carboranes. Data on the effect of the structure of carborane groups (o- or m-carboranes), methods of their introduction into adhesive compositions on the heat-resistance characteristics of glue compounds are given. It is shown that the thermal destruction of carborane-containing adhesive systems proceeds according to a different mechanism than analogous carborane-analogues. A feature of carborane-containing systems is their structuring in the 250–500°С region both in air and in an inert medium with the participation of carborane fragments of macromolecules with the formation of new, energetically strong chemical intermolecular bonds.

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Reference list

1. Petrova A.P. Povyshenie termostojkosti kleyashhih sistem na osnove fenolformaldegidnyh oligomerov pri modifikacii karboranami [Increasing thermal resistance of the adhesive systems based on phenol-formaldehyde oligomers with modification of the carborane] // Novosti materialovedeniya. Nauka i tehnika: elektron. nauch.-tehnich. zhurn. 2017. №1. St. 03. Available at: http://www.materialsnews.ru (accessed: June 27, 2017).
2. Petrova A.P., Laptev A.B. Termicheskaya ustojchivost karboransoderzhashhih kleyashhih sistem na osnove fenolformaldegidnyh oligomerov [Thermal stability of carborane containing gluing systems on the basis of formaldehyde oligomers] // Klei. Germetiki. Tehnologii. 2017. №7. S. 2–6.
3. Petrova A.P. Povyshenie termostojkosti poliuretanovyh kleyashhih sistem pri modifikacii karboranami [Increasing thermal resistance of polyurethane adhesive systems with modification of the carborane] // Novosti materialovedeniya. Nauka i tehnika: elektron. nauch.-tehnich. zhurn. 2017. №1. St. 04. Available at: http://www.materialsnews.ru (accessed: June 27, 2017).
4. Petrova A.P., Laptev A.B. Termicheskaya ustojchivost karboransoderzhashhih poliuretanovyh kleyashhih sistem [Thermal stability of carborane containing polyurethane gluing systems] // Klei. Germetiki. Tehnologii. 2017. №8. S. 2–5.
5. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] // Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
6. Kablov E.N. Aviacionnoe materialovedenie v XXI veke. Perspektivy i zadachi [Aviation materials science in the XXI century. Perspectives and tasks] // Aviacionnye materialy. Izbrannye trudy «VIAM» 1932–2002: yubil. nauch.-tehnich. sb. M.: MISIS–VIAM, 2002. S. 23–47.
7. Grashhenkov D.V., Chursova L.V. Strategiya razvitiya kompozicionnyh i funkcionalnyh materialov [Strategy of development of composite and functional materials] // Aviacionnye materialy i tehnologii. 2012. №S. S. 231–242.
8. Sharova I.A., Petrova A.P. Obzor po materialam mezhdunarodnoj konferencii po kleyam i germetikam (WAC-2012, Franciya) [Review of world adhesive and sealant conference (WAC-2012, France] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2013. №8. St. 06. Available at: http://www.viam-works.ru (accessed: June 19, 2017).
9. Grajms R. Karborany. Per. s angl. / pod red. A.F. Zhigacha [Carboranes. Trans. from Engl. / ed. by A.F. Zhigach]. M.: Mir, 1974. 264 s.
10. Petrova A.P., Valeckij P.M. Fenolno-kauchukovye karboransoderzhashhie klei s sobstvennym ferromagnetizmom [Phenolic and rubber carborane containing glues with own ferromagnetism] // Klei. Germetiki. Tehnologii. 2007. №4. S. 6–10.
11. Lipatova T.E., Bakalo L.A. Kinetika i mehanizm reakcij obrazovaniya poliuretanov [Kinetics and mechanism of reactions of education polyurethane] // Uspehi himii poliuretanov. Kiev: Naukova dumka. 1972. S. 195–213.
12. Lukina N.F., Dementeva L.A., Petrova A.P., Serezhenkov A.A. Konstrukcionnye i termostojkie klei [Constructional and heat-resistant glues] // Aviacionnye materialy i tehnologii. 2012. №S. S. 328–335.
13. Valeckij P.M., Petrova A.P. Polimernye klei na osnove karboransoderzhashhih soedinenij [Polymeric glues on the basis of carborane containing connections] // Klei. Germetiki. Tehnologii. 2005. №3. S. 2–5.
14. Petrova A.P. Magnitoprovodyashhie kleevye kompozicii na osnove karboransoderzhashhih soedinenij [Magneto conducting glue compositions on the basis of carborane containing connections] // Klei. Germetiki. Tehnologii. 2006. №11. S. 3–4.
15. Petrova A.P., Laptev A.B. Fenolno-kauchukovye klei, modificirovannye karboranami [The phenolic and rubber glues modified by carboranes] // Klei. Germetiki. Tehnologii. 2017. №6. S. 2–6.

10.

dx.doi.org/ 10.18577/2307-6046-2017-0-9-10-10

УДК 678.067.5

Vavilova M.I., Kurnosov A.O., Melnikov D.A.

Statistical processing of results target control of the prepreg of fiberglass for the assessment of stability of its production

The statistical method of control for assessment stability the process of manufactured is considered. The basics principles and series of creation the control Shukhart’s card for process operation of manufactured are described. The statistical processing results of output monitoring by mass fraction of volatile products and content of resins is carried out on example the process of production fiberglass VPS-33. The analysis of control Shukhart’s card and the assessment of controllability the technological process manufacturing of a fiberglass is carried out.

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1. Melnikov D.A., Ilichev A.V., Vavilova M.I. Sravnenie standartov dlia provedeniia mekha-nicheskikh ispytanii stekloplastikov na szhatie [Comparison of standards for carrying out mechanical tests of GRP compression strength] // Trudy VIAM: elektron. nauch.-tekhnich. zhurn. 2017. №3 (51). St. 06. Available at: http://www.viam-works.ru (accessed: June 21, 2017. DOI: 10.18577/2307-6046-2017-0-3-6-6.
2. Melekhina M.I., Kavun N.S., Rakitina V.P. Epoksidnye stekloplastiki s uluchshennoi vlago- i vodostoikostiu [Epoxy fiberglass plastics with an improved moisture and water resistance] // Aviatsionnye materialy i tekhnologii. 2013. №2. S. 29–31.
3. Kurnosov A.O., Melnikov D.A. The characteristics of fiberglass based on large deformation molten binders under conditions of the impact of operational factors // Polymer Science. Series D. 2016. Vol. 9. No. 2. P. 248–250.
4. Kablov E.N. Kontrol kachestva materialov – garantiya bezopasnosti ekspluatatsii aviatsionnoy tekhniki [Quality control of materials – security accreditation of operation of aviation engineering] // Aviatsionnye materialy i tekhnologii. 2001. №1. S. 3–8.
5. Kablov E.N. Aviakosmicheskoe materialovedenie [Aerospace materials science] // Vse materialy. Entsiklopedicheskiy spravochnik. 2008. №3. S. 2–14.
6. Raskutin A.E. Rossiiskie polimernye kompozitsionnye materialy novogo pokoleniia, ikh osvoenie i vnedrenie v perspektivnykh razrabatyvaemykh konstruktsiiakh [Russian polymer composite materials of new generation, their exploitation and implementation in advanced developed constructions] // Aviatsionnye ma-terialy i tekhnologii. 2017. №S. S. 349–367. DOI: 10.18577/2071-9140-2017-0-S-349-367.
7. Sundaron E.M. Statisticheskie metody kontrolia i upravleniia kachestvom [Statistical control methods and quality managements]: ucheb. posobie. Ulan-Ude: Izd-vo VSGTU, 2002. 54 s.
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11.

dx.doi.org/ 10.18577/2307-6046-2017-0-9-11-11

УДК 620.178.35

Grinevich A.V., Erasov V.S., Yakusheva N.A., Terekhin A.L.

Fatigue life of steel VKS-9 in conditions of symmetric loading «tension–compression» and «bending with rotation»

The article presents the results of fatigue tests of high-strength steel VKS-9, designed for use in aircraft landing gears and other highly loaded parts of aircraft. Illustrated the main difficulty in the development of high strength steels, due to the fact that the bearing capacity of structures with stress concentrators is significantly below the tensile strength, determined on a standard sample. Along with the assessment of the resistance of material to brittle fracture criterion for fatigue failure is also the basis of determining the bearing capacity. Domestic practice test for fatigue based on the loading scheme «bending and rotation». American reference books provide data on fatigue when tested according to the scheme of loading «expansion-compression». For a correct comparison of fatigue data on comparative testing of high strength steel VKS-9 at various schemes of loading. It is established that the limits of fatigue on the bases 104–106 when tested by loading the «bending-rot

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dx.doi.org/ 10.18577/2307-6046-2017-0-9-12-12

УДК 621.791.37.042.2-034.24

Titov V.I.

Determination of boron in solders based on nickel VPr24 and VPr27

As a result of the research and experimental work on the possible determination of boron content in solders based on nickel VPr24 and VPr27, a photometric analysis method was used. The main reagent was chosen H-resorcinol. Using this reagent, the reaction proceeds in a weakly acidic medium, there is no need to extract the complex formed with organic solvents. During the experiment, it was found that one of the components of the solder – niobium – interacts with the reagent H-resorcinol, thereby negatively affecting the possibility of correct determination of boron content. Masking reagent, allowing to obtain correct results of the analysis, was selected complexon III. To prevent loss of boron during the sample preparation, phosphoric acid must be added. As a result of the conducted studies, a technique for determining the boron content in the concentration range 0,1–3,0% by weight was developed in solders based on nickel VPr24 and VPr27.

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