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dx.doi.org/ 10.18577/2307-6046-2024-0-8-3-18

УДК 678.8

Gurov D.A., Tsapenko A.N., Pavlukovich N.G.

EFFECT OF MUTUAL STABILIZATION OF POLYETHERETHERKETONE AND THERMOTROPIC LIQUID CRYSTAL POLYMERS IN POLYMER COMPOSITES BASED ON THEN FOR 3D PRINTING

The effects of mutual diffusion, expressed in the nature of the temperature dependences of viscosity and other thermophysical characteristics of the melt of a filament based on polyetheretherketone (PEEK) and liquid crystal polymers (LCP), including depending on the printing speed and the content of the LC phase, are considered and substantiated. Relaxation transitions inside the fiber itself and the film obtained from it by 3D printing are characterized. It has been shown that the introduction of LCP into a thermoplastic matrix based on PEEK can stabilize the viscous behavior of the melt of a thread during its solidification.

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Reference list

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dx.doi.org/ 10.18577/2307-6046-2024-0-8-19-27

УДК 678.8

Evdokimov A.A., Gerasimov D.M., Vakhrusheva Ja.A., Venediktova M.A., Bogdan L.M.

INVESTIGATION OF THE EFFECT OF COMPONENTS ON THE PROPERTIES OF SEALING HARNESS MATERIAL FOR AUTOCLAVE MOLDING OF POLYMER COMPOSITE MATERIALS

The results of studies of the optimal component composition of the sealing harness material and the assessment of the effect of each component on the physico-mechanical characteristics of the resulting mixtures are described. Compositions based on dimethylvinylsiloxane rubber with ingredients such as covelos, carbon black and diatomite,chalk, BMK-5 copolymer and TMFT product, dicumyl peroxide are considered. Based on the conducted studies of experimental compositions, the ingredients most applicable for further development of the optimal formulation of the sealing material used in autoclave molding have been determined.

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Reference list

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dx.doi.org/ 10.18577/2307-6046-2024-0-8-28-37

УДК 621.792.053

Lukina N.F., Isaev A.Yu., Smirnov O.I., Salando R.P.

PROPERTIES OF VK-106 ADHESIVE FOR FASTENING OF HEAT-SHRINKABLE TUBES IN THE DESIGN OF ELECTRIC PLAITS

Results of research of the properties of VK-106 epoxy thixotropic adhesive intended for connection of products from heat-shrinkable materials with the shells of electric plaits and the bodies of electric connectors at melting point temperature with the subsequent curing of adhesive joint at room temperature are presented. The data on keeping of strength characteristics of the adhesive joints executed with use of VK-106 adhesive, after influence of external factors in comparison with the initial characteristics are provided.

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Reference list

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dx.doi.org/ .18577/2307-6046-2024-0-8-38-47

УДК 669.018.95

Zhelezina G.F., Kulagina G.S., Kan A.Ch., Solovjova N.A.

RESEARCH OF CORROSION RESISTANCE OF THE HYBRID LAYERED METAL POLYMERIC MATERIALS

Complex research of corrosion resistance of the hybrid layered metal polymer material «aluminum–organoplastiс» has been conducted according to the techniques accepted for different classes of materials: metals, polymer composites, adhesive compounds. It is established that the hybrid material has corrosion on surface and at the ends of the samples such as a metal alloy has. An there is also a number of features which are caused by layered structure of the metal composite, the permeability of layers of organoplastic to moisture and electrolytes.

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Reference list

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13. Arislanov A.A., Goncharova L.J., Nochovnaya N.А., Goncharov V.A. Prospects for the use of titanium alloys in laminated composite materials. Trudy VIAM, 2015, no. 10, paper no. 04. Available at: http://www.viam-works.ru (accessed: February 12, 2024). DOI: 10.18577/2307-6046-2015-0-10-4-4.
14. Kablov E.N., Startsev V.O. Effect of Internal Stresses on Aging of Polymer Composite Materials. Review. Mekhanika kompozitnykh materialov, 2021, vol. 57, no. 5, pp. 805–822.
15. Startsev O.V., Krotov A.S., Senatorova O.G., Anikhovskaya L.I., Antipov V.V., Grashchenkov D.V. Sorption and Diffusion of Moisture in Layered Metal-Polymer Composite Materials of the SIAL Type. Materialovedenie, 2011, no. 12, pp. 38–44.
16. Startsev V.O., Plotnikov V.I., Antipov Yu.V. Reversible influence of moisture on the mechanical properties of PCM after weathering. Trudy VIAM, 2018, no. 5 (65), paper no. 12. Available at: http://www.viam-works.ru (accessed: February 12, 2024). DOI: 10.18577/2307-6046-2018-0-5-110-118.
17. Aviation materials: a reference book in 13 vols. Ed. E.N. Kablov. 7th ed., add. and rev. Moscow: VIAM, 2015, vol. 13: Climatic and microbiological resistance of non-metallic materials, 270 p.
18. Kablov E.N., Startsev V.O. Systematical analysis of the climatics influence on mechanical properties of the polymer composite materials based on domestic and foreign sources (review). Aviacionnye materialy i tehnologii, 2018, no. 2 (51), pp. 47–58. DOI: 10.18577/2071-9140-2018-0-2-47-58. DOI: 10.18577/2071-9140-2018-0-2-47-58.
19. Antipov V.V., Kurs M.G., Girsh R.I., Serebrennikova N.Yu. Climatic field tests of SIAL type metal-polymer composition materials in marine climate. Aviacionnye materialy i tehnologii, 2019, no. 4 (57), pp. 56–64. DOI: 10.18577/2071-9140-2019-0-4-56-64.
20. Kablov E.N., Startsev O.V., Medvedev I.M. Review of international experience on corrosion and corrosion protection. Aviacionnye materialy i tehnologii, 2015, no. 2 (35), pp. 76–87.
21. Kablov E.N., Startsev O.V., Medvedev I.M., Panin S.V. Corrosive aggressiveness of the coastal atmosphere. Part 1. Influencing factors (review). Korroziya: materialy, zashchita, 2013, no. 12, pp. 6–18.
22. Kablov E.N., Startsev O.V., Medvedev I.M. Corrosive aggressiveness of the coastal atmosphere. Part 2. New approaches to assessing the corrosivity of coastal atmospheres. Korroziya: materialy, zashchita, 2016, no. 1, pp. 1–15.
23. Kablov E.N., Startsev V.O. Climatic aging of polymer composite materials for aviation purposes. I. Assessment of the influence of significant influencing factors. Deformatsiya i razrushenie materialov, 2019, no. 12, pp. 7–16.
24. Startsev V.O., Antipov V.V., Slavin A.V., Gorbovets M.A. Modern domestic polymer composite materials for aviation industry (review). Aviation materials and technologies, 2023, no. 2 (71), paper no. 10. Available at: http://www.journal.viam.ru (accessed: February 10, 2024). DOI: 10.18577/2713-0193-2023-0-2-122-144.
25. Startsev V.O. The degradation of polymer composite materials in seawater (review). Aviation materials and technologies, 2023, no. 1 (70), paper no. 12. (accessed: March 15, 2024). DOI: 10.185577/2713-0193-2023-0-1-148-170.
26. Method for measuring parameters of freely damped oscillations of a torsional pendulum: pat. RU 2258912 Rus. Federation; appl. 14.05.03; publ. 20.08.05.
27. Duyunova V.A., Kozlov I.A., Oglodkov M.S., Kozlova A.A. Modern trends in the anodic oxidation of aluminum-lithium and aluminum alloys (review). Trudy VIAM, 2019, no. 8 (80), paper no. 09. Available at: http://www.viam-works.ru (accessed: March 05, 2024). DOI: 10.18577/2307-6046-2019-0-8-79-89.
28. Fomina M.A., Volkov I.A., Vdovin A.I., Yamshchikov E.I. Study of protective capacity anodic oxide coating with environmental friendly improved filling technology. Aviation materials and technologies, 2023, no. 4 (73), paper no. 10. Available at: http://www.journal.viam.ru (accessed: February 12, 2024). DOI: 10.18577/2713-0193-2023-0-4-101-110.

dx.doi.org/ 10.18577/2307-6046-2024-0-8-48-63

УДК 621.352.6

Balinova Yu.A., Lugovoy A.A., Butakov V.V.

APPLICATION TRENDS OF HIGH TEMPERATURE REFRACTORY OXIDES FOR SOLID OXIDES FUEL CELLS

Solid oxide fuel cells attract the attention of developers due to their high energy efficiency, environmental friendliness and a wide variety of types of fuel used. The publication is devoted to the current state of the issue in the field of materials development for solid oxide fuel cells (SOFC). Ceramic oxide materials used for the anode, cathode and electrode of fuel cells are considered. It is shown that interest in solid oxide fuel cells will steadily grow, while small-sized SOFC up to nanoelements will have a special perspective.

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Reference list

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2. Jaiswal N., Tanwar K., Suman R. et al. A brief review on ceria based solid electrolytes for solid oxide fuel cells Journal of Alloys and Compounds, 2019, vol. 781, pp. 984–1005. DOI: 10.1016/j.jallcom.2018.12.015.
3. Zhang W., Hu Y.H. Progress in proton-conducting oxides as electrolytes for low-temperature solid oxide fuel cells: From materials to devices Energy Science and Engineering, 2021. DOI: 10.1002/ese3.886.
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8. Fan L., Zhu B., Su P.-Ch., He Ch. Nanomaterials and technologies for low temperature solid oxide fuel cells: Recent advances, challenges and opportunities Nano Energy, 2018, vol. 45, pp. 148–176. DOI: 10.1016/j.nanoen.2017.12.044.
9. Li J., Lu Y., Mushtaq N. et al. Analyzing the composite heterostructure as an efficient electrolyte for low-temperature ceramic fuel cells Journal of Alloys and Compounds, 2024, vol. 980, art. 173597. DOI: 10.1016/j.jallcom.2024.173597.
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13. Agarkov D.A., Bredikhin S.I. Solid oxide fuel cells (SOFC) and power plants based on them Energoekspert, 2021, no. 3, pp. 6–8.
14. Lyskov N.V., Kotova A.I., Petukhov D.I. et al. A new electrochemically active and stable electrode based on praseodymium molybdate for symmetric SOFCs Elektrokhimiya, 2022, vol. 58, no. 11, pp. 746–755. DOI: 10.31857/S0424857022110093.
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16. Gallyamov A.N., Kazantsev A.L., Skovorodnikov P.V., Poilov V.Z. Review of modern functional materials used in solid oxide fuel cells operating on hydrogen fuel Vestnik PNI PU. Ser.: Khimicheskaya tekhnologiya i biotekhnologiya, 2022, no. 4, pp. 38–61. DOI: 10.15593/2224-9400/2022.4.04.
17. Lomonova E.E., Kulebyakin A.V., Tabachkova N.Yu. Solid electrolytes for solid oxide fuel cells (SOFC). Available at: https://econobninsk.ru/images/prezentatsii/ИОФ_РАН_МИСИС_Ломонова_Табачкова_Твёрдые_электролиты_для_ТОТЭ_Обнинск_09-09-2021.pdf (accessed: April 19, 2024).
18. Kolchina L.M. Synthesis and high-temperature properties of multicomponent cuprates – promising cathode materials for solid oxide fuel cells: thesis, Cand. Sc. (Chem.). Moscow, 2017, 134 p.
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20. Method for producing anode substrates with a developed microstructure used in multichannel SOFCs: pat. 2777101 Rus. Federation; appl. 29.12.21; publ. 01.08.22.
21. Soloviev A.A., Sochugov N.S., Ionov I.V., Shipilova A.V., Kovalchuk A.N. Magnetron formation of Ni‒YSZ anodes of solid oxide fuel cells Elektrokhimiya, 2014, vol. 50, no. 7, pp. 724–732. DOI: 10.7868/S0424857014070160.
22. Agarkova E.A., Zadorozhnaya O.Yu., Burmistrov I.N. et al. Fabrication and electrochemical characteristics of SOFCs based on supporting two-layer anode substrates obtained by casting on a moving belt Elektrokhimiya, 2022, vol. 58, no. 2, pp. 76–84. DOI: 10.31857/S0424857022020037.
23. Simonenko T.L. Synthesis and study of solid electrolytes based on ZrO2, CeO2 and BaCe(Zr)O3 doped with magnesium, yttrium and gadolinium oxides: thesis, Cand. Sc. (Thech.). St. Petersburg, 2018, 160 p.
24. Affandi N.S.M., Osman N. Short review on global trends in SOFC scenario and future perspective Materials Today: Proceedings, 2022, vol. 66 (10), pp. 3981–3984. DOI: 10.1016/j.matpr.2022.04.824.
25. Global Solid Oxide Fuel Cell Market Share, Size, Growth, Trends, Analysis, Forecast: By Type: Planar, Tubular; By Application: Portable, Stationary, Transport; By End User: Residential, Commercial and Industrial, Data Centres, Military and Defence; Regional Analysis; Competitive Landscape; Key Trends and Developments in the Market; 2024–2032. Available at: https://markwideresearch.com/solid-oxide-fuel-cell-market/ (accessed: March 26, 2024).
26. Batista R.M., Ferreira A.M.D.C., Muccillo E.N.S. Sintering and electrical conductivity of gadolinia-doped ceria Ionics, 2016, vol. 22, pp. 1159–1166. DOI: 10.1007/s11581-016-1648-7.
27. Solovyev A.A., Rabotkin S.V., Shipilova A.V., Ionov I.V. Magnetron Sputtering of Gadolinium-doped Ceria Electrolyte for Intermediate Temperature Solid Oxide Fuel Cells International Journal of Electrochemical Science, 2019, vol. 14, pp. 575–584. DOI: 10.20964/2019.01.03.
28. Agarkov D.A. Study of the relationship between microstructure and charge transfer processes in composite electrodes of SOFCs of planar geometry: Thesis, Cand. Sc. (Phys. & Math.). Chernogolovka, 2016, 171 p.
29. Agarkov D., Borik M., Komarov B. et al. Long-Term Conductivity Stability of Electrolytic Membranes of Scandia Stabilized Zirconia Co-Doped with Ytterbia Membranes, 2023, vol. 13, p. 586. DOI: 10.3390/membranes13060586.
30. Kablov E.N., Antipov V.V. The Role of New Generation Materials in Ensuring the Technological Sovereignty of the Russian Federation Vestnik Rossiyskoy akademii nauk, 2023, vol. 93, no. 10, pp. 907–916.
31. Sokolov A.V., Deynega G.I., Kuzmina N.A. Influence of Sc2O3 additive on sintering temperature and properties of ZrO2–Y2O3 system oxide ceramics. Aviacionnye materialy i tehnologii, 2020, no. 1 (58), pp. 64–69. DOI: 10.18577/2071-9140-2020-0-1-64-69.
32. Doronin O.N., Artemenko N.I., Stekhov P.A., Voronov V.A. Deposition of ceramic layers of heat protection coatings based on the system Gd2O3–ZrO2–HfO2 and Sm2O3–Y2O3–HfO2. Aviation materials and technologies, 2022, no. 3 (68), paper no. 10. Available at: http://www.journal.viam.ru (accessed: March 26, 2024). DOI: 10.18577/2713-0193-2022-0-3-108-119.
33. Lebedeva Yu.E., Shchegoleva N.E., Voronov V.A., Solntcev S.S. Al2O3 and ZrO2 ceramic materials obtained by sol-gel method. Trudy VIAM, 2021, no. 4 (98), paper no. 05. Available at: http://www.viam-works.ru (accessed: March 26, 2024). DOI: 10.18577/2307-6046-2021-0-4-61-73.
34. Babashov V.G., Maksimov V.G., Varrik N.M., Samorodova O.N. Studying of structure and pro-perties of samples of ceramic composite materials on the basis of mullite. Aviacionnye materialy i tehnologii, 2020, no. 1 (58), pp. 54–63. DOI: 10.8577/2071-9140-2020-0-1-54-63.

dx.doi.org/ 10.18577/2307-6046-2024-0-8-64-76

УДК 666.3

Turchenko M.V., Lebedeva Yu.E., Kolmogorov A.Yu., Gurov D.A., Chaynikova A.S.

POSSIBILITY OF USING LAYER-BY-LAYER DEPOSITION TECHNOLOGY (FDM) TO PRODUCE CERAMIC PRODUCTS

When producing ceramic products with complex shapes, traditional methods cannot compete with additive manufacturing methods. This is due to both the complexity of manufacturing molds and injection molds, and the need for subsequent mechanical processing, which significantly complicates and increases the cost of the process of obtaining a product. This article discusses the layer-by-layer deposition technology (FDM). Its main advantages and disadvantages are given. The results of producing ceramic polymer filament and products made from it using FDM technology are presented.

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Reference list

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11. Kirillova N.K., Alekseeva A.N., Egorova A.D. Application of additive technologies in construction and in the manufacture of ceramic products. Vestnik Belgorodskogo gosudarstvennogo tekhnologicheskogo universiteta im. V.G. Shukhova, 2020, no. 2, pp. 131–141.
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13. Cherepanova M.V., Skovorodnikov P.V., Khazeev A.A. Application of additive technologies in the production of ceramic products of complex shapes. Nauchnyy almanakh, 2018, no. 10 (2), pp. 73–76.
14. Lakhdar Y., Tuck C., Binner J., Terry A., Goodridge R. Additive manufacturing of advanced ceramic materials. Progress in Materials Science, 2021, vol. 116, pp. 736–742.
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16. Krasheninnikov M.A. Features of additive technologies for product design. Traditions and innovations in construction and architecture. Construction technologies: collection of articles. Samara: Samara State arch.-tech. Univ, 2017, pp. 98–102.
17. Istomin A.V. Study of the distribution of aluminum oxide nanopowder in a polymer solution. Aviation materials and technologies, 2024, no. 1 (74), paper no. 06. Available at: http://www.journal.viam.ru (accessed: July 01, 2024). DOI: 10.18577/2713-0193-2024-0-1-78-88.
18. Sorokin A.E., Ivanov M.S., Sagomonova V.A. Thermoplastic polymer composite materials based on polyetheretherketones of various manufacturers. Aviation materials and technologies, 2022, no. 1 (66), paper no. 04. Available at: http://www.journal.viam.ru (accessed: July 01, 2024). DOI: 10.18577/2713-0193-2022-0-1-41-50.
19. Sokolov A.V., Deynega G.I., Kuzmina N.A. Influence of Sc2O3 additive on sintering temperature and properties of ZrO2–Y2O3 system oxide ceramics. Aviacionnye materialy i tehnologii, 2020, no. 1 (58), pp. 64–69. DOI: 10.18577/2071-9140-2020-0-1-64-69.
20. Startsev V.O., Antipov V.V., Slavin A.V., Gorbovets M.A. Modern domestic polymer composite materials for aviation industry (review). Aviation materials and technologies, 2023, no. 2 (71), paper no. 10. Available at: http://www.journal.viam.ru (accessed: July 01, 2024). DOI: 10.18577/2713-0193-2023-0-2-122-144.
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25. Smirnov A., Kuznetsova E.V., Khmyrov R.S. et al. Study of mechanical properties under tension of ceramic-polymer composites obtained by the method of layer-by-layer fusion deposition. Advanced technologies and materials: proc. Int. scientific-practical conf. (September 21–23, 2022, Sevastopol). Sevastopol: Sevastopol State Univ., 2022, pp. 199–202.
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36. Vozarova M., Neubauer E., Baca L. et al. Preparation of fully dense boron carbide ceramics by Fused Filament Fabrication (FFF). Journal of the European Ceramic Society, 2023, vol. 43, no. 5, pp. 1751–1761.

dx.doi.org/ 10.18577/2307-6046-2024-0-8-77-89

УДК 629.7.023

Fomina M.A., Sibileva S.V., Dyomin S.A., Vasiliev A.S.

THERMAL INDICATOR MATERIALS AND THEIR APPLICATION

Thermal indicators include substances that have the ability to sharply change their color at a certain temperature, called the transition temperature. These materials are of significant interest to researchers and manufacturers as they have potential for many technological applications such as aerospace, functional coatings, military applications, printing technologies, «smart» windows, temperature sensors, etc. The nomenclature and variety of thermal indicator substances are constantly evolving, as evidenced by the annual increase in scientific and technical literature publications on this topic.

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Reference list

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3. Kablov E.N. Materials and chemical technologies for aviation equipment. Vestnik Rossiyskoy akademii nauk, 2012, vol. 82, no. 6, pp. 520–530.
4. Krasnov I.S., Lozhkova D.S., Dalin M.A. Evaluation of deficiency of titanium alloy forgings for probabilistic calculation of gas turbine engine disks fracture risk. Aviation materials and technologies, 2021, no. 2 (63), paper no. 12. Available at: https: //journal.viam.ru (accessed: May 06, 2024). DOI: 10.18577/2713-0193-2021-0-2-115-122.
5. Skupov A.A., Sviridov A.V., Golev E.V., Stekolnikova E.Yu. Laser welding of heat-resistant alloy nickel base for gas turbine elements engines. Aviation materials and technologies, 2023, no. 4 (73), paper no. 01. Available at: http://www.journal.viam.ru (accessed: May 06, 2024). DOI: 10.18577/2713-0193-2023-0-4-3-13.
6. Kablov E.N., Khmeleva K.M., Zavarzin S.V., Kozlov I.A., Lonskii S.L. The effect of heat treatment on the characteristics of aluminium-zinc coatings obtained by the cold spray method. Aviation materials and technologies, 2022, no. 1 (66), paper no. 07. Available at: http://www.journal.viam.ru (ассеssed: May 06, 2024). DOI: 10.18577/2713-0193-2022-0-1-78-91.
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dx.doi.org/ 10.18577/2307-6046-2024-0-8-90-100

УДК 629.7.023.224

Gorlov D.S., Chesnokov D.V., Zaklyakova O.V., Cheredinov P.D.

THE EFFECT OF THE OPERATING MODE OF THE NEGATIVE POTENTIAL SOURCE DURING GRADIENT DEPOSITION OF THE PROTECTIVE COATING ON THE RESISTANCE TO SULFIDE OXIDE CORROSION AND SCALE RESISTANCE

The results of a study of the effect of a constant or pulse mode of operation of a negative potential inverter during gradient deposition of the protective coating of the composition SDP-1+VSDP-13 on resistance to sulfide oxide corrosion (SOC) at a temperature of 950 °С based on 30 cycles and scale resistance at a temperature of 1100 °Сbased on 200 hours are presented. It was found that the increased resistance of the «alloy–coating composition» to the effects of SOC and scale resistance are shown by coatings applied under constant operation of the inverter and with an increased potential of 70 V.

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Reference list

1. VIAM is 90 years old: We are proud of the past, we create the future. Ed. E.N. Kablov. Moscow: NRC «Kurchatov Institute» – VIAM, 2022, pp. 97–103.
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6. Echin A.B., Bondarenko Yu.A., Kolodyazhny M.Yu., Surova V.A. Review of perspective high-temperature superalloys based on refractory non-metallic materials for production of gas turbine engines. Aviation materials and technologies, 2023, no. 3 (72), paper no. 03. Available at: http://www.journal.viam.ru (accessed: June 25, 2024). DOI: 10.18577/2713-0193-2023-0-3-30-41.
7. Svetlov I.L., Petrushin N.V., Epishin A.I., Karashaew M.M., Elyutin E.S. Single crystals of nickel-based superalloys alloyed with rhenium and ruthenium (review). Part 1. Aviation materials and technologies, 2023, no. 1 (70), paper no. 03. Available at: http://www.journal.viam.ru (accessed: June 25, 2024). DOI: 10.18577/2713-0193-2023-0-1-30-50.
8. Muboyadzhyan S.A., Kablov E.N., Budinovsky S.A. Vacuum-plasma technology for producing protective coatings from complex-alloyed alloys. Metallovedenie i termicheskaya obrabotka metallov, 1995, no. 2, pp. 15–18.
9. Budinovsky S.A., Muboyadzhyan S.A. Efficiency of two-stage ion-plasma technology for producing alloyed diffusion aluminide coatings on heat-resistant nickel alloys. Metallovedenie i termicheskaya obrabotka metallov, 2003, no. 5, pp. 27–32.
10. Zavarzin S.V., Oglodkov M.S., Chesnokov D.V., Kozlov I.A. Hot corrosion and protection of materials of gas turbine engines (review). Trudy VIAM, 2018, no. 3 (109), paper no. 11. Available at: http://www.viam-works.ru (accessed: June 25, 2024). DOI: 10.18577/2307-6046-2022-0-3-121-134.
11. Kachanov E.B., Tamarin Yu.A. Coatings for protection of turbine blades from sulfide corrosion. Tekhnologiya legkikh splavov, 2005, no. 1–4, pp. 171–180.
12. Medvedev I.M., Nikitin Ya.Yu., Puzanov A.I., Laptev A.B. Hot corrosion testing methods for high-temperature alloys (review). Trudy VIAM, 2018, no. 11 (71), paper no. 11. Available at: http://www.viam-works.ru (accessed: June 25, 2024). DOI: 10.18577/2307-6046-2018-0-11-93-100.
13. Kosmin A.A., Budinovskiy S.A., Muboyadzhyan S.A. Heat and corrosion resistant coating for working turbine blades from promising high-temperature alloy VZhL21. Aviacionnye materialy i tehnologii, 2017, no. 1 (46), pp. 17–24. DOI: 10.18577/2071-9140-2017-0-1-17-24.
14. Muboyadzhyan S.A., Budinovskij S.A. Ion-plasma technology: prospective processes, coatings, equipment. Aviacionnye materialy i tehnologii, 2017, no. S, pp. 39–54. DOI: 10.18577/2071-9140-2017-0-S-39-54.
15. Budinovsky S.A., Lyapin A.A., Benklyan A.S. Pilot-industrial ion-plasma installations MESh-50 and MAP-R for applying protective coatings to parts of transport and power gas turbine units. Inzhenernyy zhurnal: nauka i innovatsii, 2021, no. 10, pp. 1–13. DOI: 10.18698/2308-6033-2021-10-2120.

dx.doi.org/ 10.18577/2307-6046-2024-0-8-101-110

УДК 543.51:669.1

Beznosyuk A.N., Alekseev A.V.

DETERMINATION OF PLATINUM GROUP ELEMENTS IN NICKEL ALLOYS BY INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY METHOD

The work determined the impurities of platinum group metals (Ru, Rh, Pd, Os, Ir, Pt) and gold in complex-alloyed nickel alloys using inductively coupled plasma mass spectrometry. The method for dissolving a sample and preparing it for analysis is presented. Spectral interferences are eliminated using a reaction-collision cell and a mathematical correction method. The accuracy of the results was confirmed by comparative analysis with data obtained using high-resolution mass spectrometry with a glow discharge.

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Reference list

1. Min P.G., Vadeev V.E., Kramer V.V. The development of the new VZhM200 superalloy and the technology of its production for casting of the advanced engines’ blades by the directional crystallization. Aviation materials and technologies, 2021, no. 3 (64), paper no. 02. Available at: http://www.journal.viam.ru (accessed: June 04, 2024). DOI: 10.18577/2713-0193-2021-0-3-11-18.
2. Kablov E.N. Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030». Aviacionnye materialy i tehnologii, 2015, no. 1 (34), pp. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
3. Min P.G., Vadeev V.E. The development and introduction into serial production of the new superalloy VZhL125 for the advanced aviation engines vanes. Aviation materials and technologies, 2023, no. 1 (70), paper no. 01. Available at: http://www.journal.viam.ru (accessed: June 04, 2024). DOI: 10.18577/2713-0193-2023-0-1-3-16.
4. Kablov E.N., Petrushin N.V., Svetlov I.L., Demonis I.M. Casting heat-resistant nickel alloys for advanced aviation gas turbine engines. Tekhnologiya legkikh splavov, 2007, no. 2, pp. 6–16.
5. Svetlov I.L., Petrushin N.V., Epishin A.I., Karashaew M.M., Elyutin E.S. Single crystals of nickel-based superalloys alloyed with rhenium and ruthenium (review). Part 1. Aviation materials and technologies, 2023, no. 1 (70), paper no. 03. Available at: http://www.journal.viam.ru (accessed: June 04, 2024). DOI: 10.18577/2713-0193-2023-0-1-30-50.
6. Svetlov I.L., Petrushin N.V., Epishin A.I., Karashaew M.M., Elyutin E.S. Single crystals of nickel-based superalloys alloyed with rhenium and ruthenium (review). Part 2. Aviation materials and technologies, 2023, no. 2 (71), paper no. 01. Available at: http://www.journal.viam.ru (accessed: June 04, 2024). DOI: 10.18577/2713-0193-2023-0-2-3-22.
7. Kablov E.N., Chabina E.B., Morozov G.A., Muravskaya N.P. Conformity assessment of new materials using high-level RMs and MI. Kompetentnost, 2017, no. 2, pp. 40–46.
8. State Standard 12228.1–78. Ruthenium. Spectral analysis method. Moscow: Publ. House of Standards, 1977, pp. 1–3.
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11. Tyutyunnik O.A., Nabiullina S.N., Anosova M.O., Kubrakova I.V. Determination of trace contents of platinum group elements and gold in ultramafic rocks using AG-X8 and LN-RESIN sorbents by inductively coupled plasma mass spectrometry. Zhurnal analiticheskoy khimii, 2020, vol. 75, no. 6, pp. 527–536.
12. Leikin A.Yu., Karandashev V.K., Lisovsky S.V., Volkov I.A. Use of a reaction-collision cell for the determination of impurity elements in rare earth metals by ICP-MS. Zavodskaya laboratoriya. Diagnostika materialov, 2014, vol. 80, no. 5, pp. 6–9.
13. Grebneva-Balyuk O.N., Kubrakova I.V. Determination of platinum group elements in geological objects by inductively coupled plasma mass spectrometry: possibilities and limitations. Zhurnal analiticheskoy khimii, 2020, vol. 75, no. 3, pp. 195–208.
14. Menshikov V.I., Vlasova V.N., Lozhkin V.I., Sokolnikova Yu.V. Determination of platinum group elements in rocks by ICP-MS with external calibration after separation of matrix elements on the KU-2-8 cation exchanger. Analytics and Control. 2016, vol. 20, no. 3, pp. 190–201.
15. Pupyshev A.A., Epova E.N. Spectral interference of polyatomic ions in the method of mass spectrometry with inductively coupled plasma. Analitika i kontrol, 2001, vol. 5, no. 4, pp. 335–369.

10.

dx.doi.org/ 10.18577/2307-6046-2024-0-8-111-120

УДК 669.018.44:669.245

Shorstov S.Yu., Dmitriev N.S., Razmakhov M.G., Skuridina N.S.

METHODOLOGICAL FEATURES OF STUDYING THE DENSITY OF METAL POWDER COMPOSITIONS AT HIGH TEMPERATURE

This paper proposes an approach to estimating the density of solid materials at elevated temperatures, based on measuring the temperature coefficient of linear expansion. Measurements of metal powder compositions of alloys EP741NP, VZh178P and VZh159 were carried out. The temperature dependences of the density of the powders under study were established in the temperature range from 200 to 1100 ºС and the correctness of the results obtained was assessed. The features of the experiment are shown, and the advantages and disadvantages of the proposed measurement method are considered.

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Reference list

1. Kablov E.N., Antipov V.V. The role of new generation materials in ensuring the technological sovereignty of the Russian Federation. Vestnik Rossiyskoy akademii nauk, 2023, vol. 93, no. 10, pp. 907–916.
2. Kablov E.N. No future without new materials. Metallurg, 2013, no. 12, рp. 4–8.
3. Kablov E.N., Bakradze M.M., Gromov V.I., Voznesenskaya N.M., Yakusheva N.A. New high strength structural and corrosion-resistant steels for aerospace equipment developed by FSUE «VIAM» (review). Aviacionnye materialy i tehnologii, 2020, no. 1 (58), pp. 3–11. DOI: 10.18577/2071-9140-2020-0-1-3-11.
4. Garibov G.S., Vostrikov A.V., Grits N.M., Fedorenko E.A. Development of new granulated heat-resistant nickel alloys for the production of disks and shafts of aircraft engines. Tekhnologiya legkikh splavov, 2010, no. 2, pp. 34–44.
5. Garibov G.S., Grits N.M. V.I. Dobatkin and metallurgy of granules of heat-resistant nickel alloys. Tekhnologiya legkikh splavov, 2015, no. 2, pp. 34–39.
6. Loshchinin Yu.V., Pakhomkin S.I., Razmakhov M.G. Phase transformation temperatures and calorimetric analysis of powder compositions of nickel-based superalloys. Aviacionnye materialy i tehnologii, 2020, no. 1 (58), pp. 79–85. DOI: 10.18577/2071-9140-2020-0-1-79-85.
7. Vostrikov A.V., Lomberg B.S., Letnikov M.N., Ovsepyan S.V. Modern heat-resistant deformable nickel alloys of VIAM for gas turbine engine parts. All-Rus. Sci. and Tech. Conf. «Modern heat-resistant deformable nickel alloys and technologies for their production». Moscow: NRC «Kurchatov Institute» – VIAM, 2021, pp. 5–14.
8. Volkov A.M., Vostrikov A.V., Bakradze M.M. Development principles and alloying features of p/m Ni-base superalloys for jet-engine disks application. Trudy VIAM, 2016, no. 8, paper no. 2. Available at: http://www.viam-works.ru (accessed: March 06, 2024). DOI: 10.18577/2307-6046-2016-0-8-2-2.
9. Sukhov D.I., Nerush S.V., Efimochkin I.Yu., Karachevchev F.N., Bogachev I.A. Production of MMC based on VZh159 alloy by selective laser melting. Aviation materials and technologies, 2021, no. 2 (63), paper no. 07. Available at: http://www.journal.viam.ru (accessed: March 06, 2024). DOI: 10.18577/2713-0193-2021-0-2-62-72.
10. Movenko D.A., Shurtakov S.V. Microcrack formation and controlling in nickel superalloys processed by selective laser melting (review). Aviation materials and technologies, 2022, no. 2 (67), paper no. 04. Available at: http://www.journal.viam.ru (accessed: March 06, 2024). DOI: 10.18577/2713-0193-2022-0-2-43-51.
11. Volkov A. M., Shestakova A. A., Bakradze M. M. The comparison of powder produced by gas atomization and by plasma rotate electrode process in the point of production disk billets from Ni-base superalloys. Trudy VIAM, 2018, no. 11 (71), paper no. 02. Available at: http://www.viam-works.ru (accessed: March 06, 2024). DOI: 10.18577/2307-6046-2018-0-11-12-19.
12. Bakradze М.М., Volkov А.М., Shestakova А.А., Letnikov M.N., Bubnov M.V. The features of the grains size changing in the p/m Ni-base superalloy for disks application produced via different technologies. Trudy VIAM, 2018, no. 2, paper no. 01. Available at: http://www.viam-works.ru (accessed: March 06, 2024). DOI: 10.18577/2307-6046-2018-0-2-1-1.
13. Koshelev V.Ya., Garibov G.S., Sukhov D.I. Basic regularities of the process of producing granules of heat-resistant alloys by plasma spraying of a rotating workpiece. Tekhnologiya legkikh splavov, 2015, no. 3, pp. 97–103.
14. Sokolovsky S.S., Astapovich O.S. Selection of the method and means for measuring the density of porous composite materials with open pores. 12th Int. Sci. and Tech. Conf. «Instrument Engineering–2019». Minsk: Belarusian National Tech. Univ., 2019, pp. 228–229.
15. Gainullin Ren.Kh., Gainullin Rish.Kh., Tsvetkova E.M. et al. Mathematical justification of the technological parameters of the device for measuring the apparent density of porous materials. Lesnoy vestnik, 2022, vol. 26, no. 4, pp. 128–134. DOI: 10.18698/2542-1468-2022-4-128-134.
16. Gainullin Ren.Kh., Gainullin Rish. Kh., Tsvetkova E.M. et al. Method for measuring the volume and determining the density of porous materials. Sistemy. Metody. Tekhnologii, 2021, no. 2 (50), pp. 106–110. DOI: 10.18324/2077-5415-2021-2-106-110.
17. Chaplygin V.Yu. Methodology for studying metal powders obtained by electrical discharge dispersion. Sovremennye materialy, tekhnika i tekhnologii, 2016, no. 1 (4), p. 225–231.
18. State Standard R 52802–2007. Heat-resistant granulated nickel alloys. Brands. Moscow: Standartinform, 2008, 10 p.
19. State Standard 5632–2014. Stainless steels and alloys, corrosion-resistant, heat-resistant and heat-resistant. Brands. Moscow: Standartinform, 2015, 57 p.
20. Kablov E.N. Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030». Aviacionnye materialy i tehnologii, 2015, no. 1 (34), pp. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.

11.

CONTENТS

Gurov D.A., Tsapenko A.N., Pavlukovich N.G. Effect of mutual stabilization of polyetheretherketone and thermotropic liquid crystal polymers in polymer composites based on them for 3D printing

Evdokimov A.A., Gerasimov D.M., Vakhrusheva Yа.A., Venediktova M.A., Bogdan L.M. Investigation of the effect of components on the properties of sealing harness material for autoclave molding of polymer composite materials

Lukina N.F., Isayev A.Yu., Smirnov O.I., Salando R.P.Properties of VK-106 adhesive for fastening of heat-shrinkable tubes in the design of electric plaits

Composite materials

Zhelezina G.F., Kulagina G.S., Kan A.Ch., Solovyova N.A.Research of corrosion resistance of the hybrid layered metal polymeric materials

Balinova Yu.A., Lugovoy A.A., Butakov V.V.Application trends of high temperature refractory oxides for solid oxides fuel cells

Turchenko M.V., Lebedeva Yu.E., Kolmogorov A.Yu., Gurov D.A., Chainikova A.S.Possibility of using layer-by-layer deposition technology (FDM) to produce ceramic products

Protective and functional

coatings

Fomina M.A., Sibileva S.V., Demin S.A., Vasiliev A.S.Thermal indicator materials and their application

Gorlov D.S., Chesnokov D.V., Zaklyakova O.V., Cheredinov P.D.The effect of the operating mode of the negative potential source during gradient deposition of the protective coating on the resistance to sulfide oxide corrosion and scale resistance

Material tests

Beznosyuk A.N., Alekseev A.V. Determination of platinum group elements in nickel alloys by inductively coupled plasma mass spectrometry method

Shorstov S.Yu., Dmitriev N.S., Razmakhov M.G., Skuridina N.S. Methodological features of studying the density of metal powder compositions at high temperature

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