Articles
A new breakthrough in the creation of new materials and technologies for producing high-nitrogen steels (HNS) in Russia was made after the installation of an electroslag remelting unit under pressure (ESRP) and the development of FGUP “VIAM” of ESRP technologies. Due to the high demands placed on semi-finished products of HNS, high requirements are also imposed on ingots of ESRP and on consumable HNS electrodes. Investigations of metal used as consumable electrodes of the ingot are conducted, and requirements for its smelting are formulated.
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6. Krylov S.A., Evgenov A.G., Shherbakov A.I., Makarov A.A. Novaya elektroshlakovaya pech pod davleniem DEShP-0,1: osvoenie i perspektivy razvitiya [New pressure electroslag remelting furnace PESR-0,1: development and prospects for improvement] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2016. №5. St. 04. Available at: http://www.viam-works.ru (accessed: May 03, 2018). DOI: 10.18577/2307-6046-2016-0-5-4-4.
7. Krylov S.A., Shcherbakov A.I., Makarov A.A., Tonysheva O.A. Snizhenie soderzhaniya nemetallicheskikh vklyuchenij v korrozionnostojkoj azotsoderzhashchej stali [Reduction of non-metallic inclusions in the nitrogen-containing corrosion-resistant steels] // Trudy VIAM: elektron. nauch.-tekhnich. zhurn. 2017. №5 (53). St. 01. Available at: http://www.viam-works.ru (accessed: May 08, 2018). DOI: 10.18577/2307-6046-2017-0-5-1-1.
8. Krylov S.A., Evgenov A.G., Makarov A.A., Tonysheva O.A. Slitok elektroshlakovogo pereplava pod davleniem [The ingot PESR] // Trudy VIAM: elektron. nauch.-tekhnich. zhurn. 2017. №3 (51). St. 03. Available at: http://www.viam-works.ru (accessed: May 10, 2018). DOI: 10.18577/2307-6046-2017-0-3-3-3.
9. Rigina L.G., Vasilev Ya.M., Dub V.S., Kolpishon E.Yu., Afanasev S.Yu. Legirovanie stali azotom [The alloying of steel with nitrogen] // Spetselektrometallurgiya. 2005. №2. S. 14–21.
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11. Kablov E.N. Innovatsionnye razrabotki FGUP «VIAM» GNTS RF po realizatsii «Strategicheskikh napravlenij razvitiya materialov i tekhnologij ikh pererabotki na period do 2030 goda» // Aviatsionnye materialy i tekhnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
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The paper studies the filtration of high-temperature nickel alloys from harmful impurities when the melt is passed through a foam ceramic filter. A microstructure was studied with the determination of the local element composition of two samples of the high-temperature nickel alloy ZhS32 with a different silicon content (0,15 and 0,32%). It is established that impurities (sulfur, silicon, oxygen) are located near and in the pores of the material, which affects the strength characteristics. A microstructural study of a master alloy sample based on Y5Si3 was carried out. As a result of x-ray phase analysis, five phases were detected: Al2Si2Y, Al3Si2Y2, Y2AlSi2, Al, Al3Y, three of which contain silicon.
2. Kablov E.N. Osnovnye itogi i napravleniya razvitiya materialov dlya perspektivnoj aviatsionnoj tekhniki [Main results and directions of development of materials for advanced aircraft technology] // 75 let. Aviacionnye materialy. Izbrannye trudy «VIAM» 1932–2007. M.: VIAM, 2007. S. 20–26.
3. Kablov E.N. Materialy novogo pokoleniya [Materials of a new generation] // Zashchita i bezopasnost'. 2014. №4. S. 28–29.
4. Kablov E.N., Petrushin N.V., Svetlov I.L., Demonis I.M. Nikelevye litejnye zharoprochnye splavy novogo pokoleniya [Nickel foundry heat resisting alloys of new generation] // Aviacionnye materialy i tehnologii. 2012. №S. C. 36–52.
5. Arzamasov V.B., Volchkov A.N., Golovin V.A. i dr. Materialovedenie i tekhnologiya konstruktsionnykh materialov [Material Science and Technology of Structural Materials.]. M.: Akademiya, 2007. 538 s.
6. Stoyakina E.A., Dyagtereva A.G. Mekhanizm udaleniya sery i fosfora iz stali U8 filtratsiej rasplava cherez penokeramiku [Mechanism of removal of sulfur and phosphorus from steel U8 by melt filtration through foam ceramics] // Politekhnicheskij molodezhnyj zhurnal MGTU im. N.E. Baumana. 2017. №12. S. 37–40.
7. Smirnov L.A., Rovnushkin V.A., Oryshchenko A.S., Kalinin G.Yu., Milyuts V.G. Modifitsirovanie stali i splavov redkozemelnymi elementami. Soobshchenie 1 [Modification of steel and alloys by rare earth elements. Message 1] // Metallurg. 2015. №11. S. 57–63.
8. Golubovskij E.R., Svetlov I.L., Petrushin N.V., CHerkasova S.A., Volkov M.E. Malotsiklovaya ustalost' monokristallov zharoprochnykh nikelevykh splavov pri povyshennykh temperaturakh [Low-cycle fatigue of single crystals of high-temperature nickel alloys at elevated temperatures] // Deformatsiya i razrushenie materialov. 2009. №8. S. 41–48.
9. Petrushin N.V., Elyutin E.S., Chabina E.B., Timofeeva O.B. O fazovykh i strukturnykh prevrashcheniyakh v zharoprochnykh renijsoderzhashchikh splavakh monokristallicheskogo stroeniya [About phase and structural transformations in heat-resistant rhenium-containing alloys of a single-crystal structure] // Litejnoe proizvodstvo. 2008. №7. S. 2–6.
10. Kablov E.N., Petrushin N.V., Svetlov I.L., Demonis I.M. Litejnye zharoprochnye nikelevye splavy dlya perspektivnykh aviatsionnykh GTD [Foundry heat-resistant nickel alloys for advanced aircraft GTE] // Tekhnologiya legkikh splavov. 2007. №2. S. 6–16.
11. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] // Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
12. Morozova G.I. Zakonomernost formirovaniya khimicheskogo sostava γ'/γ-matritsy mnogokomponentnykh nikelevykh splavov [Regularity in the formation of the chemical composition of the γ'/γ matrix of multicomponent nickel alloys] // DAN SSSR. 1991. T. 320. №6. S. 1413–1416.
13. Kablov D.E., Sidorov V.V., Min P.G., Gerasimov V.V., Bondarenko Yu. A. Vliyanie primesej sery i fosfora na svojstva monokristallov zharoprochnogo splava ZhS36-VI i razrabotka effektivnyh sposobov ego rafinirovaniya [The sulfur and phosphorus influence on properties of single crystals GHS36-VI supperalloy and design of effective methods their refining] // Aviacionnye materialy i tehnologii. 2015. №3 (36). S. 3–9. DOI: 10.18577/2071-9140-2015-0-3-3-9.
14. Min P.G., Sidorov V.V., Kablov D.E., Vadeev V.E. Issledovanie sery i fosfora v litejnykh zharoprochnykh nikelevykh splavakh i razrabotka effektivnykh sposobov ikh rafinirovaniya [Investigation of sulfur and phosphorus in foundry heat-resistant nickel alloys and development of effective methods for their refining] // Tekhnologiya metallov. 2015. №12. S. 2–9.
15. Kablov D.E., Sidorov V.V., Puchkov Yu.A. Osobennosti diffuzionnogo povedeniya primesej i rafiniruyushhih dobavok v nikele i monokristallicheskih zharoprochnyh splavah [Diffusion behavior features of impurities and microalloying additives in nickel and single crystal superalloys] // Aviacionnye materialy i tehnologii. 2016. №1 (40). S. 24–31. DOI: 10.18577/2071-9140-2016-0-1-24-31.
16. Kablov D.E., Sidorov V.V., Min P.G., Puchkov Yu.A. Vliyanie lantana na kachestvo i ekspluatacionnye svojstva monokristallicheskogo zharoprochnogo nikelevogo splava ZhS36-VI [The lanthanum influence on quality and operational properties of single crystal nickel base ZhS36-VI superalloy] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2015. №12. St. 02. Available at: http://www.viam-works.ru (accessed: August 13, 2018). DOI: 10.18577/2307-6046-2015-0-12-2-2.
17. Kablov D.E., Sidorov V.V., Min P.G., Puchkov Yu.A. Vliyanie poverhnostno-aktivnyh primesej i dobavki lantana na strukturu i svojstva monokristallicheskogo zharoprochnogo nikelevogo splava ZhS36 [Influence of surface-active impurities and lanthanum on structure and properties of singlecrystal nickel superalloy ZhS36] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2017. №4 (52). St. 02. Available at: http://www.viam-works.ru (accessed: August 13, 2018). DOI: 10.18577/2307-6046-2017-0-4-2-2.
18. Kablov D.E., Belyaev M.S., Sidorov V.V., Min P.G. Vliyanie primesej sery i fosfora na malociklovuyu ustalost monokristallov zharoprochnogo splava ZhS36-VI [The influence of sulfur and phosphorus impurities on low cycle fatigue of single crystals of ZhS36-VI alloy] // Aviacionnye materialy i tehnologii. 2015. №4 (37). S. 25–28. DOI: 10.18577/2071-9140-2015-0-4-25-28.
19. Shalin R.E., Svetlov I.L., Kachanov E.B. Monokristally nikelevykh zharoprochnykh splavov [Single crystals of nickel refractory alloys]. M.: Mashinostroenie, 1997. 336 s.
The increase in let-out volumes and especially dimensions оf products from composite, has demanded search of cheaper alternatives to avtoklave way of manufacturing of products. Ways of liquid vacuum formation dry preformеs impregnation binding have appeared the cheapest. The arisen problems of receiving high-quality products vacuum formation have led to development semi-pregs, representing fabrics or cordlike fillers which are duplicated with film of the binding. Many manufacturing firms of materials include in the nomenclature of the materials wide ruler semi-pregs. In work researches of processes of receiving polymeric composite materials (PСM) on the basis of developed semi-pregs by means of their formation by means of atmospheric pressure instead of autoclave for manufacturing of load bearing structures are considered. The interrelation of porosity of plastics, permeability, and some other parameters for the purpose of receiving PCM with minimal porosity and properties, approximate to avtoklave formation is investigated PСM.
2. Dushin M.I., Khrulkov A.V., Mukhametov R.R. Issledovanie tekhnologicheskikh parametrov avtoklavnogo formovaniya detalej iz polimernykh kompozitsionnykh materialov [Research of technological parameters of autoclave molding of parts from polymer composite materials] // Klei. Germetiki. Tekhnologii. 2013. №8. S. 12–15.
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5. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] // Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
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Protection of magnesium alloys by method of plasma electrolytic oxidation is the most perspective. Protective properties of received coverings in big degree depend on surface structure of magnesium alloy. Availability on surface of alloy the phases containing aluminum, the Mg17Al12 type leads to covering forming with large amount of through defects. Preliminary etching of magnesium alloy in solution of alkali or fluoric acid significantly reduces porosity of covering and, therefore, increases its protective properties.
2. Volkova E.F. Analiz i itogi Mezhdunarodnoj konferencii «Magnij–21. Novye gorizonty» (obzor) [The analysis and results of the International conference «Magnesium–21. Broad horizons» (review)] // Aviacionnye materialy i tehnologii. 2016. №1 (40). S. 86–94. DOI: 10.18577/2071-9140-2016-0-1-86-94.
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5. Kozlova A.A., Kondrashov Je.K. Sistemy lakokrasochnyh pokrytij dlja protivokorro-zionnoj zashhity magnievyh splavov [Systems of paint coatings for anticorrosive protection of magnesium alloys] //Aviacionnye materialy i tehnologii. 2014. №2. S. 44–47. DOI: 10.18577/2071-9140-2014-0-2-44-47.
6. Kablov E.N. Osnovnye itogi i napravleniya razvitiya materialov dlya perspektivnoj aviatsionnoj tekhniki [Main results and directions of development of materials for advanced aircraft technology] // 75 let. Aviacionnye materialy. Izbrannye trudy VIAM 1932–2007: yubil. nauch.-tekhnich. sb. M.: VIAM, 2007. S. 20–26.
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8. Vladimirov B.V., Krit B.L., Morozova N.V., Epelfeld A.V. Issledovanie svojstv modifitsirovannogo magnievogo splava MA21, prednaznachennogo dlya ispolzovaniya v biosensornykh sistemakh [Investigation of the properties of the modified magnesium alloy MA21, intended for use in biosensor systems] // Biotekhnologiya i kachestvo zhizni: materialy Mezhdunar. nauch.-praktich. konf. 2014. S. 179–180.
9. Kozlov I.A., Vinogradov S.S., Naprienko S.A. Struktura i svojstva PEO-pokrytiya, formiruemogo na splave ML5 v silikatno-fosfatnom elektrolite [Structure and properties of the PEO coating formed on the ML5 alloy in a silicate-phosphate electrolyte] // Korroziya: materialy, zashchita. 2017. №8. S. 35–41.
10. Rakoch A.G., Gladkova A.A., Schneider O. i dr. Vliyanie katodnykh mikrorazryadov na skorost' obrazovaniya i stroenie pokrytij, formiruemykh na magnievom splave metodom plazmenno-elektroliticheskogo oksidirovaniya [Influence of cathode microdischarges on the rate of formation and structure of coatings formed on a magnesium alloy by the plasma-electrolytic oxidation method] // Perspektivnye materialy. 2014. №5. S. 59–64.
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13. Kozlov I.A., Vinogradov S.S., Kulyushina N.V. Vliyanie formy polyarizuyushchikh impulsov na strukturu i zashchitnye svojstva PEO-pokrytiya, formiruemogo na splave ML5 [Influence of the form of the polarizing impulses on structure and protective properties PEO coating formed on alloy ML5] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2017. №8 (56). St. 12. Available at: http://www.viam-works.ru (accessed: April 16, 2018). DOI: 10.18577/2307-6046-2017-0-8-12-12.
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Materials of structural elements of aircraft gas turbine engines during operation are subjected to a wide range of static and dynamic loads in a wide range of operating temperatures and durability. Therefore, to calculate the strength of the main parts of the engine and confirm their service life, it is necessary to have a large range of strength characteristics of metal materials under static and cyclic loading. The paper presents an overview of the characteristics of the strain-controlled low-cycle fatigue, obtained on Walter+Bai machines.
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Novel carbon fiber reinforced plastics VKU-27l, VKU-39, VKU-46 and glass reinforced plastics VPS-47/7781, VPS-48/7781, based on VST-1208, VSE-1212, VSR-3M resigns in initial state and after 12 month of weathering in warm and mild cold climate were investigated by means of profilometry, diffusion analysis and dynamical mechanical analysis. The influence of material composition on mean size of sample surface inhomogeneities, moisture content, diffusion coefficient, glass transition temperature of resigns was studied. The physicomechanical transitions were studied at the early stage of natural weathering.
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12. Nikolaev E.V., Barbotko S.L., Andreeva N.P., Pavlov M.R., Grashchenkov D.V. Kompleksnoe issledovanie vozdejstviya klimaticheskih i ekspluatacionnyh faktorov na novoe pokolenie epoksidnogo svyazuyushhego i polimernyh kompozicionnyh materialov na ego osnove. Chast 3. Raschet energii aktivacii i teplovogo resursa polimernyh kompozicionnyh materialov na osnove epoksidnoj matricy [Comprehensive research of the influence of climatic and operational factors on new generation epoxy binding and polymeric composite materials on its basis Part 3. Calculation of activation energy and thermal resource of polymeric composite materials on the basis of epoxy matrix] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2016. №5. St. 11. Available at: http://www.viam-works.ru (accessed: June, 25 2018). DOI: 10.18577/2307-6046-2016-0-5-11-11.
13. Nikolaev E.V., Barbotko S.L., Andreeva N.P., Pavlov M.R., Grash-chenkov D.V. Kompleksnoe issledovanie vozdeystviya klimaticheskikh i ekspluatatsionnykh faktorov na novoe pokolenie epoksidnogo svyazuyushchego i polimernykh kompozitsionnykh materialov na ego osnove. Chast 4. Naturnye klimaticheskie ispytaniya polimernykh kompozitsionnykh materialov na osnove epoksidnoy matritsy [Complex research of influence of climatic and operational factors on new generation epoxy binding and polymeric composite materials on its basis. Part 4. Natural climatic tests of polymeric composite materials on the basis of epoxy matrix] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2016. №6. St. 11. Available at: http://www.viam-works.ru (accessed: June, 25 2018). DOI: 10.18577/2307-6046-2016-0-6-11-11.
14. Mishurov K.S., Pavlovskij K.A., Imametdinov E.SH. Vliyanie vneshnej sredy na svojstva ugleplastika VKU-27L [Environmental effects on properties of CFRP (carbon fiber reinforced plastic) VKU-27L] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2018. №3 (63). St. 07. Available at: http://www.viam-works.ru (accessed: June, 25 2018). DOI: 10.18577/2307-6046-2018-0-3-60-67.
15. Nikolaev E.V., Pavlov M.R., Laptev A.B., Ponomarenko S.A. K voprosu opredeleniya sorbi-rovannoj vlagi v polimernyh kompozitsionnyh materialah [To the problem of determining the moisture sorbed in polymeric composite materials] // Trudy VIAM: elektron. nauch.-tekhnich. zhurn. 2017. №8 (56). St. 07. Available at: http://www.viam-works.ru (accessed: June, 25 2018). DOI: 10.18577/2307-6046-2017-0-8-7-7.
16. Startsev V.O., Mahonkov A.Yu., Kotova E.A. Mehanicheskie svojstva i vlagostojkost' PKM s povrezhdeniyami [Mechanical properties and moisture resistance of PCM with damages] // Aviacionnye materialy i tehnologii. 2015. №S1 (38). S. 49–55. DOI: 10.18577/2071-9140-2015-0-S1-49-55.
17. Startsev V.O., Panin S.V., Startsev O.V. Sorption and diffusion of moisture in polymer composite materials with drop-weight impact damage // Mechanics of Composite Materials. 2016. Vol. 51. No. 6. P. 761–770.
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19. Perov N.S., Startsev V.O., Chutskova E.Yu., Gulyaev A.I., Abramov D.V. Svojstva ugleplastika na osnove politsianuratnogo svyazuyushchego posle ekspozitsii v razlichnykh estestvennykh i iskusstvennykh sredakh [Properties of carbon-based plastics on the basis of a polycyanurate binder after exposure in various natural and artificial environments] // Materialovedenie. 2017. №2. S. 3–9.
20. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] // Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
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The article describes the various methods of static loading constructive-like specimen of a hybrid welded wing-skin panel for determining of strength characteristics. It is determined that selection of optimal loading method is influenced by the necessity of structure element resistance force determination or zone hybrid elements, the shear stress level in the design, test equipment and test complexity possible. It is shown that for the hybrid and welded panel zone investigation, including the quality and stability bonding technology determination, is preferred by bending loading scheme. Testing equipment is proposed in the form of two identical supports and a loading tip with rounded contact surfaces for three-point bending test of constructive-like specimen of a hybrid welded wing-skin panel with longitudinal stringers. Using the developed equipment allows bending loading for constructive-like specimen of a hybrid welded wing-skin panel both along the stringer and across. The sustainability of the constructive-like specimen hybrid wing-skin panels in three-point bending test using proposed testing equipment is provided by fixing the stringers and preventing the local crumpling and brittle fracture of the hybrid laminate strips during the test by reducing the contact stresses.
2. Oreshko E.I., Erasov V.S., Podzhivotov N.Yu., Lutsenko A.N. Raschet na prochnost gibridnoj paneli kryla na baze listov i profilej iz vysokoprochnogo alyuminijlitievogo splava i sloistogo alyumostekloplastika [Strength calculation of hybrid wing panel on the basis of sheets and profiles from high-strength aluminum lithium alloy and laminated aluminum fiberglass] // Aviacionnye materialy i tehnologii. 2016. №1 (40). S. 53–61. DOI: 10.18577/2071-9140-2016-0-1-53-61.
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11. Device for preventing metal welded joint bending test samples from deviating in test process: pat. 203479602 U China. №CN20132512200U; pub. 12.03.14.
12. Tool for testing bending performance of carbon fiber composite material of T-shaped beam: pat. 204101369 U China. №CN20142654406U; pub. 14.01.15.
13. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] // Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
14. Erasov V.S., Yakovlev N.O., Nuzhnyj G.A. Kvalifikatsionnye ispytaniya i issledovaniya prochnosti aviatsionnyh materialov [Qualification tests and researches of durability of aviation materials] // Aviacionnye materialy i tehnologii. 2012. №S. S. 440–448.
15. Osnastka dlya ispytanij na izgib konstruktivno-podobnykh obraztsov gibridnoj paneli kryla: pat. 262685 C2 Ros. Federatsiya. №2015144207 [Rigging tool for constructively similar samples of a hybrid wing panel: pat. 262685 C2 Ros. Federation. №2015144207]; zayavl. 15.10.15; opubl. 18.07.17, Byul. №20. 10 s
The article presents advantages strain-controlled testing over force-controlled testing at static tension and repeated-static (fatigue) with a fixed deformation step. In addition to the traditional mechanical properties of materials (elastic modulus E, yield strength σ0,2, tensile strength σв, permanent deformation δ), obtained from the stress-strain diagram at tensile test, introduction of additional characteristics (plastic deformation rate
, material damage function of the specimen ω, damage velocity ) subject to stress-strain diagram with strain-controlled testing is suggested. The stress-strain diagram relationship with the envelope of the line when the strain-controlled repeated-static testing with a fixed deformation step introduced. Approaches to determining fatigue characteristics using test data in this manner at fatigue testing are showing. For 1441-T1 and 1163-ATB alloys under repeated-static testing, a characteristic effect is observe. A plastic deformation in a certain deformation range is realize discretely at the same stresses (similar to the yield plateau during tension). For alloy B-1481-T1, there is no similar effect.
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Anodic dissolution of aluminum alloys in different solutions was studied as a promising approach to imitate corrosion of these alloys in natural environment. The solution, containing sodium nitrate, sodium sulfite and sodium chloride with «Ekomet» additive, which allows formation of pitting corrosion damage, comparable to observed in natural environment, during the anodic polarization, was developed. To promote not only the pitting corrosion, but also intergranular and exfoliation corrosion, additional chlorides were added to the solution. Alternative approach is to perform anodic dissolution in solution, containing nitrates, sulfites and
chlorides, first and then in sulfite-chloride solution.
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The results of the determination of the thermal conductivity and heat capacity of epoxy material directly during its curing, are given. when the phase state changes. As an object of research, an epoxy formulation based on epoxy-diane resin and modified aliphatic polyamine was used. Thermophysical properties were determined for different degrees of conversion at room and elevated temperatures. Depending on the degree of conversion, the value of volumetric shrinkage and residual stresses were also evaluated. It was found that during the curing process (i.e., when the degree of conversion is changed), the heat capacity decreases by 32% and more than three times the thermal conductivity increase.
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